[2-(4-Nitrophenyl)-2-oxoethyl] 5-bromofuran-2-carboxylate

Base Information

Chemical Name:[2-(4-Nitrophenyl)-2-oxoethyl] 5-bromofuran-2-carboxylate
CAS No.:5528-13-2
Molecular Formula:C13H8BrNO6
Molecular Weight:167.164
Hs Code.:
DSSTox Substance ID:DTXSID60360298
Wikidata:Q82141968

Synonyms:5528-13-2;DTXSID60360298;[2-(4-nitrophenyl)-2-oxoethyl] 5-bromofuran-2-carboxylate;AKOS000741417;AB00087470-01;SR-01000513467;SR-01000513467-1;2-(4-NITROPHENYL)-2-OXOETHYL 5-BROMO-2-FUROATE

Suppliers and Price of [2-(4-Nitrophenyl)-2-oxoethyl] 5-bromofuran-2-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of [2-(4-Nitrophenyl)-2-oxoethyl] 5-bromofuran-2-carboxylate

Chemical Property:

Vapor Pressure:7.73E-11mmHg at 25°C
Boiling Point:518.1°Cat760mmHg
Flash Point:267.1°C
Density:1.654g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:352.95350
Heavy Atom Count:21
Complexity:415

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C(=O)COC(=O)C2=CC=C(O2)Br)[N+](=O)[O-]

Technology Process of [2-(4-Nitrophenyl)-2-oxoethyl] 5-bromofuran-2-carboxylate

There total 6 articles about [2-(4-Nitrophenyl)-2-oxoethyl] 5-bromofuran-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.1%

: 3328-77-6
1-(2,4-dihydroxy-5-nitrophenyl)ethanone

: 5528-13-2
1-(5-amino-2,4-dihydroxyphenyl)ethanone

Guidance literature:: With sodium dithionite; water; In methanol; for 2h; Reflux;
DOI:10.1007/s00044-018-2139-3

Reference yield:

: 5528-13-2
1-(5-amino-2,4-dihydroxyphenyl)ethanone

Guidance literature:: With nickel; acetone; Hydrogenation;
DOI:10.1021/ja01283a013

Reference yield:

: 108-46-3
recorcinol

: 5528-13-2
1-(5-amino-2,4-dihydroxyphenyl)ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: zinc(II) chloride / 0.5 h / 140 °C

2: acetic acid; nitric acid / 7 h / 20 °C

3: sodium dithionite; water / methanol / 2 h / Reflux

With sodium dithionite; water; nitric acid; acetic acid; zinc(II) chloride; In methanol;
DOI:10.1007/s00044-018-2139-3