Phosphorous acid, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-phenylpropyl dimethyl ester

Base Information

Chemical Name:Phosphorous acid, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-phenylpropyl dimethyl ester
CAS No.:137333-84-7
Molecular Formula:C₁₇H₃₁O₄PSi
Molecular Weight:358.49
Hs Code.:

Synonyms:

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Chemical Property of Phosphorous acid, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-phenylpropyl dimethyl ester

Chemical Property:

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Technology Process of Phosphorous acid, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-phenylpropyl dimethyl ester

There total 4 articles about Phosphorous acid, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-phenylpropyl dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21915-53-7,40641-81-4,91465-28-0,98819-67-1,98819-68-2,99528-63-9,104196-23-8,105663-44-3,116661-35-9
2,3-epoxy-3-phenyl-1-propanol

: 137333-84-7
1-phenyl-3-<(tert-butyldimethylsilyl)oxy>propyl dimethyl phosphite

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Red-Al / Sharpless reaction

2: 93 percent / pyridine

3: tetrazole / acetonitrile / Ambient temperature

With pyridine; 1H-tetrazole; sodium bis(2-methoxyethoxy)aluminium dihydride; In acetonitrile;
DOI:10.1021/jo00026a008

Reference yield:

: 104-54-1
3-Phenylpropenol

: 137333-84-7
1-phenyl-3-<(tert-butyldimethylsilyl)oxy>propyl dimethyl phosphite

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / mCPBA

2: 96 percent / Red-Al / Sharpless reaction

3: 93 percent / pyridine

4: tetrazole / acetonitrile / Ambient temperature

With pyridine; 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; In acetonitrile;
DOI:10.1021/jo00026a008

Reference yield:

: 4850-49-1
1-phenyl-1,3-propanediol

: 137333-84-7
1-phenyl-3-<(tert-butyldimethylsilyl)oxy>propyl dimethyl phosphite

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / pyridine

2: tetrazole / acetonitrile / Ambient temperature

With pyridine; 1H-tetrazole; In acetonitrile;
DOI:10.1021/jo00026a008