OM 46

Base Information

• Chemical Name: OM 46
• CAS No.: 55380-75-1
• Molecular Formula: 2C₇H₈O₃S*C₂₂H₃₃N₅O₄S
• Molecular Weight: 808.011
• Mol file: 55380-75-1.mol

Synonyms:

Chemical Property of OM 46

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of OM 46

There total 3 articles about OM 46 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

toluene-4-sulfonic acid (104-15-4) + Nα-dansyl-L-arginine (4307-78-2,28217-22-3,71869-46-0) + butan-1-ol (71-36-3) → Nα-dansyl-L-arginine n-butyl ester bis(p-toluenesulfonate) (55380-75-1)

Guidance literature:

In benzene; for 3h; Heating;

DOI:10.1021/jm00182a003

Reference yield:

5-(dimethylamino)naphth-1-ylsulfonyl chloride (605-65-2) → Nα-dansyl-L-arginine n-butyl ester bis(p-toluenesulfonate) (55380-75-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / K₂CO₃ / H₂O; diethyl ether / 48 h / Ambient temperature

2: 95 percent / benzene / 3 h / Heating

With potassium carbonate; In diethyl ether; water; benzene;

DOI:10.1021/jm00182a003

Reference yield:

L-arginine (74-79-3,157-06-2,7004-12-8,7200-25-1,25212-18-4) → Nα-dansyl-L-arginine n-butyl ester bis(p-toluenesulfonate) (55380-75-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / K₂CO₃ / H₂O; diethyl ether / 48 h / Ambient temperature

2: 95 percent / benzene / 3 h / Heating

With potassium carbonate; In diethyl ether; water; benzene;

DOI:10.1021/jm00182a003

upstream raw materials:

toluene-4-sulfonic acid

N^α-dansyl-L-arginine

butan-1-ol

5-(dimethylamino)naphth-1-ylsulfonyl chloride