6,6-dimethyl-1-{3-[(phenylsulfanyl)methyl]phenyl}-1,6-dihydro-1,3,5-triazine-2,4-diamine

Base Information

Chemical Name:6,6-dimethyl-1-{3-[(phenylsulfanyl)methyl]phenyl}-1,6-dihydro-1,3,5-triazine-2,4-diamine
CAS No.:87739-40-0
Molecular Formula:C₁₈H₂₁N₅S*ClH
Molecular Weight:375.925
Hs Code.:

Synonyms:1,3,5-Triazine-2,4-diamine,1,6-dihydro-6,6-dimethyl-1-[3-[(phenylthio)methyl]phenyl]-, monohydrochloride(9CI)

Suppliers and Price of 6,6-dimethyl-1-{3-[(phenylsulfanyl)methyl]phenyl}-1,6-dihydro-1,3,5-triazine-2,4-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of 6,6-dimethyl-1-{3-[(phenylsulfanyl)methyl]phenyl}-1,6-dihydro-1,3,5-triazine-2,4-diamine

Chemical Property:

Vapor Pressure:3.9E-11mmHg at 25°C
Boiling Point:525.5°Cat760mmHg
Flash Point:271.6°C
Density:1.26g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6,6-dimethyl-1-{3-[(phenylsulfanyl)methyl]phenyl}-1,6-dihydro-1,3,5-triazine-2,4-diamine

There total 4 articles about 6,6-dimethyl-1-{3-[(phenylsulfanyl)methyl]phenyl}-1,6-dihydro-1,3,5-triazine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 80239-80-1
3-<(phenylthio)methyl>aniline hydrochloride

: 127099-85-8,780722-26-1,461-58-5
N-Cyanoguanidine

: 67-64-1
acetone

: 87739-40-0
4,6-diamino-1,2-dihydro-2,2-dimethyl-1-<3-<(phenylthio)methyl>phenyl>-s-triazine hydrochloride

Guidance literature:: for 20h; Heating;
DOI:10.1021/jm00344a013

Reference yield:

: 108-98-5
thiophenol

: 87739-40-0
4,6-diamino-1,2-dihydro-2,2-dimethyl-1-<3-<(phenylthio)methyl>phenyl>-s-triazine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / potassium carbonate / acetone / 48 h / Heating

2: 1.) acetic acid, iron, 2.) HCl gas / 1.) H₂O, 85-95 deg C, 10 h, 2.) ether

3: 95 percent / 20 h / Heating

With hydrogenchloride; iron; potassium carbonate; acetic acid; In acetone;
DOI:10.1021/jm00344a013

Reference yield:

: 619-23-8
3-Nitrobenzyl chloride

: 87739-40-0
4,6-diamino-1,2-dihydro-2,2-dimethyl-1-<3-<(phenylthio)methyl>phenyl>-s-triazine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / potassium carbonate / acetone / 48 h / Heating

2: 1.) acetic acid, iron, 2.) HCl gas / 1.) H₂O, 85-95 deg C, 10 h, 2.) ether

3: 95 percent / 20 h / Heating

With hydrogenchloride; iron; potassium carbonate; acetic acid; In acetone;
DOI:10.1021/jm00344a013