9-[3,5-O-(1-methylethylidene)pentofuranosyl]-9H-purin-6-amine

Base Information

Chemical Name:9-[3,5-O-(1-methylethylidene)pentofuranosyl]-9H-purin-6-amine
CAS No.:7687-49-2
Molecular Formula:C13H17 N5 O4
Molecular Weight:307.3052
Hs Code.:

Synonyms:Adenine,9-(3,5-O-isopropylidene-b-D-xylofuranosyl)- (7CI,8CI); 4H-Furo[3,2-d]-1,3-dioxin, 9H-purin-6-aminederiv.; NSC 79494

Suppliers and Price of 9-[3,5-O-(1-methylethylidene)pentofuranosyl]-9H-purin-6-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 9-[3,5-O-(1-methylethylidene)pentofuranosyl]-9H-purin-6-amine

Chemical Property:

Vapor Pressure:1.1E-14mmHg at 25°C
Boiling Point:588.3°Cat760mmHg
Flash Point:309.6°C
Density:1.8g/cm³

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 9-[3,5-O-(1-methylethylidene)pentofuranosyl]-9H-purin-6-amine

There total 4 articles about 9-[3,5-O-(1-methylethylidene)pentofuranosyl]-9H-purin-6-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 67-64-1
acetone

: 524-69-6
adenine xyloside

: 7687-49-2
9-(3,5-O-isopropylidene-β-D-xylofuranosyl)adenine

Guidance literature:: With hydrogenchloride; orthoformic acid triethyl ester; In N,N-dimethyl-formamide; for 168h; Ambient temperature;
DOI:10.1021/jm00356a010

Reference yield:

: 5432-87-1
1,2,3,5-tetra-O-benzoyl-α-D-xylofuranose

: 7687-49-2
9-(3,5-O-isopropylidene-β-D-xylofuranosyl)adenine

Guidance literature:: Multi-step reaction with 3 steps

1: HBr; acetic acid; 1,2-dichloroethane / Erhitzen des Reaktionsprodukts mit 6-Benzoylamino-purin-9-ylquecksilber-chlorid in Xylol

2: methanol. sodium methylate

3: unter Zusatz von CuSO₄ in Methansulfonsaeure und Aethansulfonsaeure

With hydrogen bromide; sodium methylate; acetic acid; 1,2-dichloro-ethane;
DOI:10.1021/jo01359a028

Reference yield:

: 125322-67-0
N-benzoyl-9-(2,3,5-tri-O-benzoyl-D-xylofuranosyl)adenine

: 7687-49-2
9-(3,5-O-isopropylidene-β-D-xylofuranosyl)adenine

Guidance literature:: Multi-step reaction with 2 steps

1: methanol. sodium methylate

2: unter Zusatz von CuSO₄ in Methansulfonsaeure und Aethansulfonsaeure

With sodium methylate;
DOI:10.1021/jo01359a028