Amorphane

Base Information

• Chemical Name: Amorphane
• CAS No.: 13833-20-0
• Molecular Formula: C15H28
• DSSTox Substance ID: DTXSID00275099
• Nikkaji Number: J38.577H
• Mol file: 13833-20-0.mol

Synonyms:Amorphane;Muurolane;decahydro-1,6-dimethyl-4-(1-methylethyl)naphthalene;Muurolane-B;13833-20-0;DTXSID00275099;FZZNNPQZDRVKLU-UHFFFAOYSA-N;29788-41-8;4-Isopropyl-1,6-dimethyldecahydronaphthalene #;34315-85-0

Chemical Property of Amorphane

Chemical Property:

• XLogP3: 6.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 208.219100893
• Heavy Atom Count: 15
• Complexity: 206

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1CCC2C(CCC(C2C1)C(C)C)C

Technology Process of Amorphane

There total 27 articles about Amorphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.5%

γ-muurolene (24268-39-1) → cis-cadinane (483-73-8,6980-47-8,10208-82-9,11011-77-1,13833-20-0,20479-38-3,20479-39-4,20479-40-7,20479-52-1,20479-53-2,20479-54-3,29788-41-8,34315-85-0,46385-68-6,46385-69-7,46385-71-1,71030-06-3,119565-03-6)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethyl acetate;

DOI:10.1016/S0040-4039(00)81749-9

Reference yield:

6-isopropyl-9-methyl-deca-1,7t,9-trien-3-ol (67910-68-3) → cis-cadinane (483-73-8,6980-47-8,10208-82-9,11011-77-1,13833-20-0,20479-38-3,20479-39-4,20479-40-7,20479-52-1,20479-53-2,20479-54-3,29788-41-8,34315-85-0,46385-68-6,46385-69-7,46385-71-1,71030-06-3,119565-03-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 77.7 percent / H₂CrO₇ / diethyl ether / 0 °C

2: 80.2 percent / tetrahydrofuran / -20 °C

3: 95.5 percent / H₂ / PtO₂ / ethyl acetate

With hydrogen; dichromic acid; platinum(IV) oxide; In tetrahydrofuran; diethyl ether; ethyl acetate;

DOI:10.1016/S0040-4039(00)81749-9

Reference yield:

6-methyl-4-(1'-methylethyl)-3,4,4a,7,8,8a-hexahydro-1(2H)-naphthalenone (28080-03-7,67910-69-4,71252-49-8,71252-50-1,87141-41-1,94425-73-7) → cis-cadinane (483-73-8,6980-47-8,10208-82-9,11011-77-1,13833-20-0,20479-38-3,20479-39-4,20479-40-7,20479-52-1,20479-53-2,20479-54-3,29788-41-8,34315-85-0,46385-68-6,46385-69-7,46385-71-1,71030-06-3,119565-03-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 80.2 percent / tetrahydrofuran / -20 °C

2: 95.5 percent / H₂ / PtO₂ / ethyl acetate

With hydrogen; platinum(IV) oxide; In tetrahydrofuran; ethyl acetate;

DOI:10.1016/S0040-4039(00)81749-9

upstream raw materials:

(+)-10-epi-zonarene

(1R,10R)-zonarene

ethanol

4-isopropenyl-1-methyl-6-methylene-decahydro-naphthalene

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