Ethenetricarbonitrile, (4-hydroxy-2,3,5-trimethylphenyl)-

Base Information

• Chemical Name: Ethenetricarbonitrile, (4-hydroxy-2,3,5-trimethylphenyl)-
• CAS No.: 138385-50-9
• Molecular Formula: C14H11N3O
• Molecular Weight: 237.261
• Mol file: 138385-50-9.mol

Synonyms:

Chemical Property of Ethenetricarbonitrile, (4-hydroxy-2,3,5-trimethylphenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Ethenetricarbonitrile, (4-hydroxy-2,3,5-trimethylphenyl)-

There total 1 articles about Ethenetricarbonitrile, (4-hydroxy-2,3,5-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

2,3,5-Trimethyl-1,4-benzoquinone (935-92-2) + malononitrile (109-77-3) → 2,3,5-trimethyl-4-oxo-2,5-cyclohexadiene-1-ylidenepropanedinitrile (123849-28-5) + 2-Cyano-3-(4-hydroxy-2,3,5-trimethyl-phenyl)-but-2-enedinitrile (138385-50-9)

Guidance literature:

With pyridine; titanium tetrachloride; In dichloromethane; at 20 ℃; for 15h; Yields of byproduct given;

DOI:10.1021/jo00032a017

upstream raw materials:

2,3,5-Trimethyl-1,4-benzoquinone

malononitrile

Refernces