tertiary-butyloxycarbonyl-alanine imidazolide

Base Information

Chemical Name:tertiary-butyloxycarbonyl-alanine imidazolide
CAS No.:86194-94-7
Molecular Formula:C₁₁H₁₇N₃O₃
Molecular Weight:239.274
Hs Code.:2933290090
Mol file:86194-94-7.mol

Synonyms:Carbamicacid, [2-(1H-imidazol-1-yl)-1-methyl-2-oxoethyl]-, 1,1-dimethylethyl ester, (?à)-;N-[N-(tert-Butoxycarbonyl)-DL-alanyl]imidazole

Suppliers and Price of tertiary-butyloxycarbonyl-alanine imidazolide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of tertiary-butyloxycarbonyl-alanine imidazolide

Chemical Property:

PSA：84.22000
Density:1.43g/cm³
LogP:0.57030

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tertiary-butyloxycarbonyl-alanine imidazolide

There total 6 articles about tertiary-butyloxycarbonyl-alanine imidazolide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 15761-38-3
L-N-Boc-Ala

: 530-62-1
1,1'-carbonyldiimidazole

: 54430-64-7,86194-94-7,92008-48-5
[(1S)-2-imidazol-1-yl-1-methyl-2-oxo-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1039/b510756c

Reference yield:

: 3744-87-4,7764-95-6,15761-38-3
N-t-butyloxycarbonyl-DL-alanine

: 530-62-1
1,1'-carbonyldiimidazole

: 86194-94-7
(2-Imidazol-1-yl-1-methyl-2-oxo-ethyl)-carbamic acid tert-butyl ester

Guidance literature:: In tetrahydrofuran; for 0.5h; Ambient temperature;
DOI:10.1016/S0040-4020(01)88730-5

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 86194-94-7
(2-Imidazol-1-yl-1-methyl-2-oxo-ethyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90.5 percent / aq. NaOH / dioxane / 0.5 h / Ambient temperature

2: tetrahydrofuran / 0.5 h / Ambient temperature

With sodium hydroxide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1016/S0040-4020(01)88730-5