1,1'-Thiocarbonyldiimidazole

Base Information

Chemical Name:1,1'-Thiocarbonyldiimidazole
CAS No.:6160-65-2
Molecular Formula:C9H16N2O
Molecular Weight:178.217
Hs Code.:29332900
European Community (EC) Number:228-183-4
NSC Number:141692
UNII:H8A75XB5AY
DSSTox Substance ID:DTXSID70210614
Nikkaji Number:J5.204C
Wikipedia:Thiocarbonyldiimidazole
Wikidata:Q2161003
Mol file:6160-65-2.mol

Synonyms:1,1'-thiocarbonyldiimidazole

Suppliers and Price of 1,1'-Thiocarbonyldiimidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AHH
1,1-Thiocarbonyldiimidazole 97%
500g
$ 735.00

AK Scientific
N,N'-Thiocarbonyldiimidazole(TCDI),tech.
100g
$ 220.00

Alfa Aesar
1,1'-Thiocarbonyldiimidazole, tech 90%
50g
$ 319.00

Alfa Aesar
1,1'-Thiocarbonyldiimidazole, tech 90%
250g
$ 1039.00

Alfa Aesar
1,1'-Thiocarbonyldiimidazole, tech 90%
10g
$ 95.10

TRC
1,1’-Thiocarbonyldiimidazole
25g
$ 360.00

TCI Chemical
1,1'-Thiocarbonyldiimidazole >95.0%(GC)(T)
5g
$ 45.00

TCI Chemical
1,1'-Thiocarbonyldiimidazole >95.0%(GC)(T)
25g
$ 221.00

SynQuest Laboratories
1,1'-Thiocarbonyldi(1H-imidazole) 95%
250 g
$ 413.00

SynQuest Laboratories
1,1'-Thiocarbonyldi(1H-imidazole) 95%
25 g
$ 64.00

Total 180 raw suppliers

Chemical Property of 1,1'-Thiocarbonyldiimidazole

Chemical Property:

Appearance/Colour:yellow powder
Melting Point:98-102 °C(lit.)
Refractive Index:1.5500 (estimate)
Boiling Point:390.8 °C at 760 mmHg
PKA:1.96±0.10(Predicted)
Flash Point:190.1 °C
PSA：67.73000
Density:1.39 g/cm³
LogP:0.76090
Storage Temp.:2-8°C
Sensitive.:Moisture Sensitive
Solubility.:Soluble in terahydrofuran, toluene and dichloromethane.
Water Solubility.:decomposes
XLogP3:0.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:178.03131738
Heavy Atom Count:12
Complexity:166

Purity/Quality:

99% ^*data from raw suppliers

1,1-Thiocarbonyldiimidazole 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 22-34
Safety Statements: 22-24/25-45-36/37/39-26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Chemical Classes:Nitrogen Compounds -> Imidazoles
Canonical SMILES:C1=CN(C=N1)C(=S)N2C=CN=C2
Uses 1,1’Thiocarbonyldiimidazole can be used to deoxygenate carboxylic monosaccharide analogues. 1,1'-Thiocarbonyldiimidazole is used as a reagent for the deoxygenation of alcohols with tributyltin hydride and diols with lithium aluminum hydride. It is also used to deoxygenate carboxylic monosaccharide analogues. Further, it is a useful reagent involved in biochemical synthesis. In addition to this, it is used to prepare 1-[bis-(4-methoxy-phenyl)-methyl]-1H-imidazole by reacting with 4,4'-dimethoxy-benzhydrol.

Technology Process of 1,1'-Thiocarbonyldiimidazole

There total 3 articles about 1,1'-Thiocarbonyldiimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%