1,3,4-Oxadiazole-2(3H)-thione, 5-(3,5-dibromo-2-hydroxyphenyl)-3-(((2,6-dichlorophenyl)amino)methyl)-

Base Information

Chemical Name:1,3,4-Oxadiazole-2(3H)-thione, 5-(3,5-dibromo-2-hydroxyphenyl)-3-(((2,6-dichlorophenyl)amino)methyl)-
CAS No.:81963-79-3
Molecular Formula:C₁₅H₉Br₂Cl₂N₃O₂S
Molecular Weight:526.035
Hs Code.:
Mol file:81963-79-3.mol

Synonyms:BRN 4592342;1,3,4-Oxadiazole-2(3H)-thione, 5-(3,5-dibromo-2-hydroxyphenyl)-3-(((2,6-dichlorophenyl)amino)methyl)-;81963-79-3;C15H9Br2Cl2N3O2S;C15-H9-Br2-Cl2-N3-O2-S;LS-99194

Suppliers and Price of 1,3,4-Oxadiazole-2(3H)-thione, 5-(3,5-dibromo-2-hydroxyphenyl)-3-(((2,6-dichlorophenyl)amino)methyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,3,4-OXADIAZOLE-2(3H)-THIONE, 5-(3,5-DIBROMO-2-HYDROXYPHENYL)-3-(((2, 6-DICHLOROPHENYL)AMINO)METHYL)- 95.00%
5MG
$ 495.78

Total 0 raw suppliers

Chemical Property of 1,3,4-Oxadiazole-2(3H)-thione, 5-(3,5-dibromo-2-hydroxyphenyl)-3-(((2,6-dichlorophenyl)amino)methyl)-

Chemical Property:

Vapor Pressure:3.77E-10mmHg at 25°C
Boiling Point:500.5°Cat760mmHg
Flash Point:256.5°C
PSA：95.05000
Density:2.03g/cm³
LogP:5.16020
XLogP3:6.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:524.81388
Heavy Atom Count:25
Complexity:535

Purity/Quality:: 1,3,4-OXADIAZOLE-2(3H)-THIONE, 5-(3,5-DIBROMO-2-HYDROXYPHENYL)-3-(((2, 6-DICHLOROPHENYL)AMINO)METHYL)- 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)Cl)NCN2C(=S)OC(=N2)C3=C(C(=CC(=C3)Br)Br)O)Cl

Technology Process of 1,3,4-Oxadiazole-2(3H)-thione, 5-(3,5-dibromo-2-hydroxyphenyl)-3-(((2,6-dichlorophenyl)amino)methyl)-

There total 4 articles about 1,3,4-Oxadiazole-2(3H)-thione, 5-(3,5-dibromo-2-hydroxyphenyl)-3-(((2,6-dichlorophenyl)amino)methyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 81963-76-0
5-(2-Hydroxy-3,5-dibromophenyl)-1,3,5-oxadiazole-2-thione

: 608-31-1
2,6-Dichloroaniline

: 81963-79-3
5-(3,5-Dibromo-2-hydroxy-phenyl)-3-[(2,6-dichloro-phenylamino)-methyl]-3H-[1,3,4]oxadiazole-2-thione

Guidance literature:: In ethanol; for 1h;
DOI:10.1002/jhet.5570190103

Reference yield:

: 21702-79-4
3,5-dibromo-2-hydroxymethyl benzoate

: 81963-79-3
5-(3,5-Dibromo-2-hydroxy-phenyl)-3-[(2,6-dichloro-phenylamino)-methyl]-3H-[1,3,4]oxadiazole-2-thione

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / 60percent hydrazine hydrate / methanol / 0.33 h / Heating

2: 70 percent / ethanol / Heating

3: 60 percent / ethanol / 1 h

With hydrazine hydrate; In methanol; ethanol;
DOI:10.1002/jhet.5570190103

Reference yield:

: 119-36-8,8024-54-2
methyl salicylate

: 81963-79-3
5-(3,5-Dibromo-2-hydroxy-phenyl)-3-[(2,6-dichloro-phenylamino)-methyl]-3H-[1,3,4]oxadiazole-2-thione

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / Br₂ / acetic acid / 1 h / Ambient temperature

2: 80 percent / 60percent hydrazine hydrate / methanol / 0.33 h / Heating

3: 70 percent / ethanol / Heating

4: 60 percent / ethanol / 1 h

With bromine; hydrazine hydrate; In methanol; ethanol; acetic acid;
DOI:10.1002/jhet.5570190103