Technology Process of Germane, hydroxytrimethyl-
There total 1 articles about Germane, hydroxytrimethyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
methanol; acetonitrile;
byproducts: PhCH2CH2COOMe, PhCH2CH(OMe)2; Electrolysis; in MeOH/MeCN (1/9, v/v) + KOH soln. in MeOH, 30 mA/cm**2 with stirring; evapd. dissolved (Et2O), washed (H2O), GC-MS, NMR;
DOI:10.1016/j.jorganchem.2011.12.025
- Guidance literature:
-
In
tetrachloromethane; water;
an aliquot of aq. soln. containing varius concens. of hydrohalogenic acid and germanium compd. is shaken with an aliquot of CCl4 for 30 min in a centrifuge tube at 25°C; after phase sepn., the germanium concen. in both the phases is determined with an inductivity coupled argon plasma emission spectrometer;
Kinetics;
DOI:10.1246/bcsj.64.3363
- Guidance literature:
-
In
tetrachloromethane; water;
aq. soln. containing hydrohalogenic acid and a dried ion-exchange resin are placed in a centrifuge tube, addn. of germanium compd., shaking gently for 24 h at 25°C; resin is sepd. by filteration and shaken with aq. NaOH for 24 h to elute the germanium compd.; the germanium compd. concens. in hydrohalogenic acid and the elute is determined with the ICAP-500;
Kinetics;
DOI:10.1246/bcsj.64.3363