Butanoic acid, 3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-[(2-hydroxyethyl)amino]-4-oxo -, phenylmethyl ester, (S)-

Base Information

Chemical Name:Butanoic acid, 3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-[(2-hydroxyethyl)amino]-4-oxo -, phenylmethyl ester, (S)-
CAS No.:138582-71-5
Molecular Formula:C₁₈H₂₆N₂O₆
Molecular Weight:366.414
Hs Code.:

Synonyms:

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Chemical Property of Butanoic acid, 3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-[(2-hydroxyethyl)amino]-4-oxo -, phenylmethyl ester, (S)-

Chemical Property:

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Technology Process of Butanoic acid, 3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-[(2-hydroxyethyl)amino]-4-oxo -, phenylmethyl ester, (S)-

There total 4 articles about Butanoic acid, 3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-[(2-hydroxyethyl)amino]-4-oxo -, phenylmethyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 138582-71-5
(S)-3-tert-Butoxycarbonylamino-N-(2-hydroxy-ethyl)-succinamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / aq. NaOH / dioxane

2: N-methyl-morpholine / tetrahydrofuran / -20 °C

3: tetrahydrofuran

With 4-methyl-morpholine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1016/0040-4039(91)80242-X

Reference yield:

: 2177-63-1,25248-99-1
(S)-2-amino-4-(benzyloxy)-4-oxobutanoic acid

: 138582-71-5
(S)-3-tert-Butoxycarbonylamino-N-(2-hydroxy-ethyl)-succinamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / aq. NaOH / dioxane

2: N-methyl-morpholine / tetrahydrofuran / -20 °C

3: tetrahydrofuran

With 4-methyl-morpholine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1016/0040-4039(91)80242-X

Reference yield:

: 7536-58-5,98482-77-0
BOC-L-aspartic acid 4-benzyl ester

: 138582-71-5
(S)-3-tert-Butoxycarbonylamino-N-(2-hydroxy-ethyl)-succinamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-methyl-morpholine / tetrahydrofuran / -20 °C

2: tetrahydrofuran

With 4-methyl-morpholine; In tetrahydrofuran;
DOI:10.1016/0040-4039(91)80242-X