ETHYL 2-(2,4-DICHLOROANILINO)-2-OXOACETATE

Base Information

• Chemical Name: ETHYL 2-(2,4-DICHLOROANILINO)-2-OXOACETATE
• CAS No.: 15313-47-0
• Molecular Formula: C10H9 Cl2 N O3
• Molecular Weight: 262.092
• Hs Code.: 2924299090
• Mol file: 15313-47-0.mol

Synonyms:Aceticacid, [(2,4-dichlorophenyl)amino]oxo-, ethyl ester (9CI); Oxanilic acid,2',4'-dichloro-, ethyl ester (8CI); NSC 406136

Chemical Property of ETHYL 2-(2,4-DICHLOROANILINO)-2-OXOACETATE

Chemical Property:

• Melting Point: 116-118°C
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 55.40000
• Density: 1.432g/cm³
• LogP: 2.56800

Purity/Quality:

99% ^*data from raw suppliers

Ethyl 2-(2,4-dichloroanilino)-2-oxoacetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL 2-(2,4-DICHLOROANILINO)-2-OXOACETATE

There total 3 articles about ETHYL 2-(2,4-DICHLOROANILINO)-2-OXOACETATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,4-Dichloroaniline (554-00-7,51908-09-9) + Ethyl oxalyl chloride (4755-77-5) → ethyl 2-(2,4-dichloroanilino)-2-oxo-acetate (15313-47-0)

Guidance literature:

With triethylamine; In dichloromethane; for 24h; Heating;

DOI:10.1080/10426500211717

Reference yield:

2,4-Dichloroaniline (554-00-7,51908-09-9) + oxalic acid diethyl ester (95-92-1) → ethyl 2-(2,4-dichloroanilino)-2-oxo-acetate (15313-47-0)

Guidance literature:

at 180 - 200 ℃;

Reference yield:

→ ethyl 2-(2,4-dichloroanilino)-2-oxo-acetate (15313-47-0)

Guidance literature:

Oxalsaeure-diethylester, 2,4-Dichloranilin;

DOI:10.1021/je60062a005

upstream raw materials:

2,4-Dichloroaniline

oxalic acid diethyl ester

Ethyl oxalyl chloride

Downstream raw materials:

N-(2,4-Dichlor-phenyl)-oxaminsaeure-hydrazid

N'-(2-Diaethylamino-aethyl)-N-(2,4-dichlor-phenyl)-oxamid

N'-(4-Diaethylamino-1-methyl-butyl)-N-(2,4-dichlor-phenyl)-oxamid

ethyl(2,4-dichlorophenylamino)hydroxyiminoacetate