1-Phenylethyl hydrogen phthalate

Base Information

Chemical Name:1-Phenylethyl hydrogen phthalate
CAS No.:33533-53-8
Molecular Formula:C16H14O4
Molecular Weight:270.285
Hs Code.:
Mol file:33533-53-8.mol

Synonyms:1-Phenyl-cyclobutanol-(1);Benzene,cyclobut-1-yl-1-ol;1-phenylcyclobutanol;1-phenyl-1-cyclobutanol;(+-)-phthalic acid mono-(1-phenyl-ethyl ester);Cyclobutanol,1-phenyl;1-phenylethyl acid phthalate;1-phenylethyl hydrogenphthalate;phenylcyclobutanol;

Suppliers and Price of 1-Phenylethyl hydrogen phthalate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1,2-BenzenedicarboxylicAcidMono(1-phenylethyl)Ester
100mg
$ 75.00

Sigma-Aldrich
PHTHALIC ACID MONO-(1-PHENYL-ETHYL) ESTER Aldrich
1ea
$ 57.00

ChemScene
1,2-Benzenedicarboxylicacid,mono(1-phenylethyl)ester
5g
$ 125.00

Total 7 raw suppliers

Chemical Property of 1-Phenylethyl hydrogen phthalate

Chemical Property:

Vapor Pressure:1.96E-08mmHg at 25°C
Melting Point:83-84 °C
Boiling Point:437.7°Cat760mmHg
PKA:3.34±0.36(Predicted)
Flash Point:162.7°C
PSA：63.60000
Density:1.24g/cm³
LogP:3.30280

Purity/Quality:

≥95% ^*data from raw suppliers

1,2-BenzenedicarboxylicAcidMono(1-phenylethyl)Ester ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Phenylethyl hydrogen phthalate

There total 5 articles about 1-Phenylethyl hydrogen phthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 85-44-9
phthalic anhydride

: 98-85-1,13323-81-4
1-Phenylethanol

: 33533-53-8,17470-31-4
(+/-)-α-methylbenzyl hydrogen phthalate

Guidance literature:: With (-)-(S)-N,N-dimethyl-1-phenylethylamine; for 36h; Ambient temperature;

Reference yield:

: 85-44-9
phthalic anhydride

: 33533-53-8,17470-31-4
(+/-)-α-methylbenzyl hydrogen phthalate

Guidance literature:: at 115 ℃;

Reference yield:

: 100-52-7
benzaldehyde

: 33533-53-8,17470-31-4
(+/-)-α-methylbenzyl hydrogen phthalate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: pyridine

With pyridine; diethyl ether;
DOI:10.1039/jr9300002260