Benzenesulfonamide, N-[(butylamino)carbonyl]-4-chloro-

Base Information

• Chemical Name: Benzenesulfonamide, N-[(butylamino)carbonyl]-4-chloro-
• CAS No.: 13909-64-3
• Molecular Formula: C11H15ClN2O3S
• Molecular Weight: 290.771
• DSSTox Substance ID: DTXSID00392896
• Nikkaji Number: J1.575.241F
• Mol file: 13909-64-3.mol

Synonyms:13909-64-3;Benzenesulfonamide, N-[(butylamino)carbonyl]-4-chloro-;DTXSID00392896;AKOS024345815;CCG-357658;N-[(Butylamino)carbonyl]-4-chlorobenzenesulfonamide;Z425552856;1-((((BUTYLAMINO)CARBONYL)AMINO)SULFONYL)-4-CHLOROBENZENE

Chemical Property of Benzenesulfonamide, N-[(butylamino)carbonyl]-4-chloro-

Chemical Property:

• XLogP3: 2.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 290.0491912
• Heavy Atom Count: 18
• Complexity: 359

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCNC(=O)NS(=O)(=O)C1=CC=C(C=C1)Cl

Technology Process of Benzenesulfonamide, N-[(butylamino)carbonyl]-4-chloro-

There total 5 articles about Benzenesulfonamide, N-[(butylamino)carbonyl]-4-chloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

4-Chlorobenzenesulfonamide (98-64-6) + n-butyl isocyanide (111-36-4) → N-(butylcarbamoyl)-4-chlorobenzenesulfonamide (13909-64-3)

Guidance literature:

With copper(l) chloride; In nitromethane; at 20 ℃; for 2h; Milling;

DOI:10.1039/c3cc47905f

Reference yield:

4-chlorobenzenesulfonamide methanoic acid ethyl ester (13945-53-4) + N-butylamine (109-73-9,85404-21-3) → N-(butylcarbamoyl)-4-chlorobenzenesulfonamide (13909-64-3)

Guidance literature:

DOI:10.1021/jo01100a622

Reference yield:

N,N'-di-n-butylurea (1792-17-2) + Natrium-(4-chlor-benzolsulfonsaeureamid) (18522-94-6,91512-11-7) → N-(butylcarbamoyl)-4-chlorobenzenesulfonamide (13909-64-3)

Guidance literature:

at 180 ℃;

DOI:10.1039/j39670000701

upstream raw materials:

4-chlorobenzenesulfonamide methanoic acid ethyl ester

N-butylamine

N,N'-di-n-butylurea

Natrium-(4-chlor-benzolsulfonsaeureamid)