Benzoic acid, 4-chloro-, 2-hydroxyheptyl ester, (S)-

Base Information

Chemical Name:Benzoic acid, 4-chloro-, 2-hydroxyheptyl ester, (S)-
CAS No.:141356-77-6
Molecular Formula:C₁₄H₁₉ClO₃
Molecular Weight:270.756
Hs Code.:

Synonyms:

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Chemical Property of Benzoic acid, 4-chloro-, 2-hydroxyheptyl ester, (S)-

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Technology Process of Benzoic acid, 4-chloro-, 2-hydroxyheptyl ester, (S)-

There total 8 articles about Benzoic acid, 4-chloro-, 2-hydroxyheptyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141339-60-8
4-Chloro-benzoic acid 2-oxo-heptyl ester

: 141356-77-6
(S)-2-hydroxyheptyl 4-chlorobenzoate

Guidance literature:: With D-glucose; immobilized baker's yeast; In water; at 35 ℃; for 72h; Yield given;
DOI:10.1246/bcsj.65.631

Reference yield:

: 201230-82-2
carbon monoxide

: (Z)-hex-1-en-1-yl 4-chlorobenzoate

: (S)-1-hydroxyheptan-2-yl 4-chlorobenzoate

: 141356-77-6
(S)-2-hydroxyheptyl 4-chlorobenzoate

Guidance literature:: carbon monoxide; (Z)-hex-1-en-1-yl 4-chlorobenzoate; With 2,2',2'',2'''-(1,2-phenylenebis((1S,3S)-tetrahydro-5,8-dioxo-1H-(1,2,4)diazaphospholo(1,2-a)pyridazine-2,1,3(3H)-triyl))tetrakis(N-(1S)-1-phenylethyl)-benzamide; acetylacetonatodicarbonylrhodium(l); hydrogen; In tetrahydrofuran; at 60 ℃; for 24h; under 8258.9 Torr; Glovebox; Inert atmosphere; Schlenk technique;

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 0 ℃; enantioselective reaction; Glovebox; Inert atmosphere; Schlenk technique;
DOI:10.1021/ja507701k

Reference yield:

: 41055-92-9
1-chloro-2-heptanone

: 141356-77-6
(S)-2-hydroxyheptyl 4-chlorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / tetrabutylammonium bromide / benzene / 3 h / Heating

2: immobilized baker's yeast, glucose / H₂O / 72 h / 35 °C

With D-glucose; immobilized baker's yeast; tetrabutylammomium bromide; In water; benzene;
DOI:10.1246/bcsj.65.631