Silane, [2-(3-chlorophenyl)ethenyl]trimethyl-, (E)-

Base Information

Chemical Name:Silane, [2-(3-chlorophenyl)ethenyl]trimethyl-, (E)-
CAS No.:141381-24-0
Molecular Formula:C₁₁H₁₅ClSi
Molecular Weight:210.779
Hs Code.:

Synonyms:

Suppliers and Price of Silane, [2-(3-chlorophenyl)ethenyl]trimethyl-, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Silane, [2-(3-chlorophenyl)ethenyl]trimethyl-, (E)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Silane, [2-(3-chlorophenyl)ethenyl]trimethyl-, (E)-

There total 4 articles about Silane, [2-(3-chlorophenyl)ethenyl]trimethyl-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 766-83-6
m-chlorophenylacetylene

: 141381-24-0
(E)-1-(m-chlorophenyl)-2-(trimethylsilyl)ethene

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethylzinc / hexane; acetonitrile / 1 h / 80 °C

1.2: 20 h

2.1: diisobutylaluminium hydride / hexane / 0 - 20 °C / Inert atmosphere

With diethylzinc; diisobutylaluminium hydride; In hexane; acetonitrile;
DOI:10.1021/acs.joc.1c02734

Reference yield:

: 625-99-0
3-iodochlorobenzene

: 18107-18-1
diazomethyl-trimethyl-silane

: C₁₁H₁₅ClSi

: 141381-24-0
(E)-1-(m-chlorophenyl)-2-(trimethylsilyl)ethene

Guidance literature:: With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; potassium acetate; lithium tert-butoxide; catacxium A; In 1,4-dioxane; at 100 ℃; for 24h; Overall yield = 42%; Overall yield = 44 mg; stereoselective reaction; Inert atmosphere;
DOI:10.1039/C8CC07664B