2H-Furo[2,3-b][1,4]diazepin-2-one, 8-cyclohexyl-8,8a-dihydro-3-(hydroxydiphenylgermyl)-8a-methoxy-5-(4- methoxyphenyl)-

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Chemical Name:2H-Furo[2,3-b][1,4]diazepin-2-one, 8-cyclohexyl-8,8a-dihydro-3-(hydroxydiphenylgermyl)-8a-methoxy-5-(4- methoxyphenyl)-
CAS No.:141784-61-4
Molecular Formula:C33H34GeN2O5
Molecular Weight:611.233
Hs Code.:

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Chemical Property of 2H-Furo[2,3-b][1,4]diazepin-2-one, 8-cyclohexyl-8,8a-dihydro-3-(hydroxydiphenylgermyl)-8a-methoxy-5-(4- methoxyphenyl)-

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Technology Process of 2H-Furo[2,3-b][1,4]diazepin-2-one, 8-cyclohexyl-8,8a-dihydro-3-(hydroxydiphenylgermyl)-8a-methoxy-5-(4- methoxyphenyl)-

There total 1 articles about 2H-Furo[2,3-b][1,4]diazepin-2-one, 8-cyclohexyl-8,8a-dihydro-3-(hydroxydiphenylgermyl)-8a-methoxy-5-(4- methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 134408-14-3
HN(C₆H₁₁)CHCHC(C₆H₄OCH₃)NH

: 762-42-5
dimethyl acetylenedicarboxylate

: 1613-66-7
dichlorodiphenylgermane

: 141784-61-4
(Ge(OH)(C₆H₅)2)CC(O)OC(OCH₃)N(C₆H₁₁)CHCHC(C₆H₄OCH₃)NC

Guidance literature:: With 1,8-diazabicyclo{5.4.0}undec-7-ene; In toluene; slow addn. of dichlorogermanium-compd. in toluene to the butadiene-compd. and DBU in toluene, stirring overnight at room temp., addn. of DMAD, stirring at room temp. for 24 h; pouring into ice-cooled 1 M H2SO4, extn. with ether, washing with H2O, drying over Na2SO4, evapn. (reduced pressure), column chromy. (silica gel, hexane-ether 2:1); elem. anal.;
DOI:10.1021/om00043a013