2-Propenoic acid, 2-methyl-3-[1-[2-[methyl(2-phenylethyl)amino]-2-oxoethyl]-5-(phenylmeth oxy)-1H-indol-3-yl]-, ethyl ester

Base Information

Chemical Name:2-Propenoic acid, 2-methyl-3-[1-[2-[methyl(2-phenylethyl)amino]-2-oxoethyl]-5-(phenylmeth oxy)-1H-indol-3-yl]-, ethyl ester
CAS No.:141835-25-8
Molecular Formula:C32H34N2O4
Molecular Weight:510.633
Hs Code.:
Mol file:141835-25-8.mol

Synonyms:

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Chemical Property of 2-Propenoic acid, 2-methyl-3-[1-[2-[methyl(2-phenylethyl)amino]-2-oxoethyl]-5-(phenylmeth oxy)-1H-indol-3-yl]-, ethyl ester

Chemical Property:

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Technology Process of 2-Propenoic acid, 2-methyl-3-[1-[2-[methyl(2-phenylethyl)amino]-2-oxoethyl]-5-(phenylmeth oxy)-1H-indol-3-yl]-, ethyl ester

There total 3 articles about 2-Propenoic acid, 2-methyl-3-[1-[2-[methyl(2-phenylethyl)amino]-2-oxoethyl]-5-(phenylmeth oxy)-1H-indol-3-yl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 589-08-2
N-Methyl-N-phenethylamine

: 141835-25-8
(E)-3-{5-Benzyloxy-1-[(methyl-phenethyl-carbamoyl)-methyl]-1H-indol-3-yl}-2-methyl-acrylic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / CH₂Cl₂ / -25 - 20 °C

2: 1.) NaH / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 18 h

3: 1.) NaH / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 5 h

With sodium hydride; In dichloromethane;
DOI:10.1021/jm950699x

Reference yield:

: 6953-22-6
5-benzyloxyindole-3-carboxaldehyde

: 141835-25-8
(E)-3-{5-Benzyloxy-1-[(methyl-phenethyl-carbamoyl)-methyl]-1H-indol-3-yl}-2-methyl-acrylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 18 h

2: 1.) NaH / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 5 h

With sodium hydride;
DOI:10.1021/jm950699x

Reference yield:

: 73391-97-6
N-methyl-N-2-phenylethyl-2-bromoacetamide

: 141835-25-8
(E)-3-{5-Benzyloxy-1-[(methyl-phenethyl-carbamoyl)-methyl]-1H-indol-3-yl}-2-methyl-acrylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 18 h

2: 1.) NaH / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 5 h

With sodium hydride;
DOI:10.1021/jm950699x