Benzeneacetic acid, a-methyl-, 4-methoxyphenyl ester, (S)-

Base Information

Chemical Name:Benzeneacetic acid, a-methyl-, 4-methoxyphenyl ester, (S)-
CAS No.:141964-53-6
Molecular Formula:C₁₆H₁₆O₃
Molecular Weight:256.301
Hs Code.:

Synonyms:

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Chemical Property of Benzeneacetic acid, a-methyl-, 4-methoxyphenyl ester, (S)-

Chemical Property:

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Technology Process of Benzeneacetic acid, a-methyl-, 4-methoxyphenyl ester, (S)-

There total 4 articles about Benzeneacetic acid, a-methyl-, 4-methoxyphenyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3893-35-4
1-diazo-1-phenyl-2-propanone

: 150-76-5
4-methoxy-phenol

: 1308679-17-5
4-methoxyphenyl (R)-2-phenylpropanoate

: 141964-53-6
(S)-4-methoxyphenyl 2-phenylpropanoate

Guidance literature:: With C₁₂H₁₄N₂S; In 2-methyltetrahydrofuran; at 40 ℃; for 16h; Overall yield = 72 percent; enantioselective reaction; Inert atmosphere; Schlenk technique; Irradiation;
DOI:10.1021/acs.orglett.9b03227

Reference yield:

: 36065-28-8
(2S)-1-(4-methoxyphenyl)-2-phenylpropan-1-one

: 141964-53-6
(S)-4-methoxyphenyl 2-phenylpropanoate

: 141964-52-5
(S)-1-phenylethan-1-yl 4'-methoxybenzoate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 20 ℃; for 720h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(00)80275-X

Reference yield:

: 15231-78-4
2.2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione

: 1308679-17-5
4-methoxyphenyl (R)-2-phenylpropanoate

: 141964-53-6
(S)-4-methoxyphenyl 2-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

2: cesium chloride; potassium phosphate; (R)-2,10-di-tert-butyl-3,9-dimethoxy-6-methyl-6-(1-naphthalen-1-ylethyl)-4,8-bis(3,4,5-trifluorophenyl)-6,7-dihydro-5H-dibenzo[c,e]-azepinium bromide / 48 h / 20 °C / Inert atmosphere

With potassium phosphate; (R)-2,10-di-tert-butyl-3,9-dimethoxy-6-methyl-6-(1-naphthalen-1-ylethyl)-4,8-bis(3,4,5-trifluorophenyl)-6,7-dihydro-5H-dibenzo[c,e]-azepinium bromide; cesium chloride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201800331