Adenosine, N-benzoyl-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-, 2'-(hydrogen phosphonate), compd. with N,N-diethylethanamine (1:1)

Base Information

Chemical Name:Adenosine, N-benzoyl-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-, 2'-(hydrogen phosphonate), compd. with N,N-diethylethanamine (1:1)
CAS No.:142025-16-9
Molecular Formula:C₆H₁₅N*C₂₉H₄₄N₅O₈PSi₂
Molecular Weight:779.034
Hs Code.:

Adenosine,
N-benzoyl-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-,
2'-(hydrogen phosphonate), compd. with N,N-diethylethanamine (1:1)

Synonyms:

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Chemical Property of Adenosine, N-benzoyl-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-, 2'-(hydrogen phosphonate), compd. with N,N-diethylethanamine (1:1)

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Technology Process of Adenosine, N-benzoyl-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-, 2'-(hydrogen phosphonate), compd. with N,N-diethylethanamine (1:1)

There total 1 articles about Adenosine, N-benzoyl-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-, 2'-(hydrogen phosphonate), compd. with N,N-diethylethanamine (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 15715-58-9
triethylamine carbonate

: 79154-57-7
3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-N₆-benzoyladenosine

: 142025-16-9
N⁶-benzoyl-3',5'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine-2'-(hydrogenphosphonate), triethylammonium salt

Guidance literature:: With 4-methyl-morpholine; 1,2,4-Triazole; phosphorus trichloride; 1) CH₂Cl₂, 0 deg C, 10 min, 2) H₂O;
DOI:10.1016/S0040-4020(01)92259-8

Reference yield:

: 135732-99-9
N⁶-benzoyl-2',3'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine

: 142025-16-9
N⁶-benzoyl-3',5'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine-2'-(hydrogenphosphonate), triethylammonium salt

: 142025-22-7
N⁶-benzoyl-3',5'-O-(1,1,3,3-tetraisopropyl-1,3-disilanediyl)-(S_P)-P-thioadenylyl-(2'-5')-N⁶-benzoyl-2',3'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine, triethylammonium salt

: (R_P)-N⁶-benzoyl-3'-O-(t.butyldimethylsilyl)-5'-O-(dimethoxytrityl)-P-thioadenylyl-(2'-5')-N⁶-benzoyl-2',3'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine, triethylammonium salt

Guidance literature:: With pyridine; pivaloyl chloride; sulfur; Yield given. Multistep reaction. Yields of byproduct given; 1) RT, 30 min;
DOI:10.1016/S0040-4020(01)92259-8