Boranediamine, N,N'-bis[2,6-bis(1-methylethyl)phenyl]-N,N'-dimethyl-

Base Information

Chemical Name:Boranediamine, N,N'-bis[2,6-bis(1-methylethyl)phenyl]-N,N'-dimethyl-
CAS No.:142039-16-5
Molecular Formula:C₂₆H₄₁BN₂
Molecular Weight:392.436
Hs Code.:

Synonyms:

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Chemical Property of Boranediamine, N,N'-bis[2,6-bis(1-methylethyl)phenyl]-N,N'-dimethyl-

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Technology Process of Boranediamine, N,N'-bis[2,6-bis(1-methylethyl)phenyl]-N,N'-dimethyl-

There total 5 articles about Boranediamine, N,N'-bis[2,6-bis(1-methylethyl)phenyl]-N,N'-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 16853-85-3
lithium aluminium tetrahydride

: 142039-19-8
bis{(2,6-diisopropylphenyl)methylamino}fluoroborane

: 142039-16-5
bis{(2,6-diisopropylphenyl)methylamino}borane

Guidance literature:: In diethyl ether; N2 atmosphere; addn. of suspn. of B-compd. in Et2O to LiAlH4 in Et2O, refluxing (2 h); sepn. of salts, removal of Et2O, crystn. (Et2O/hexane), drying (vac.);

Reference yield: 25.0%

: 142039-14-3
{(2,6-diisopropylphenyl)methylamino}difluoroborane

: 142039-16-5
bis{(2,6-diisopropylphenyl)methylamino}borane

Guidance literature:: With Na/K; naphthalene; In hexane; N2 atmosphere; addn. of org. compd. to suspn. of Na/K alloy in hexane with stirring, refluxing (3 h), addn. of B-compd., refluxing (6 h); removal of solvent (vac.), distn.; elem. anal.;

Reference yield: 13.0%

: 110-71-4
1,2-dimethoxyethane

: 142039-14-3
{(2,6-diisopropylphenyl)methylamino}difluoroborane

: 142039-16-5
bis{(2,6-diisopropylphenyl)methylamino}borane

: 142039-15-4
{(2,6-diisopropylphenyl)methylamino}dimethoxyborane

: 142039-18-7
bis({(2,6-diisopropylphenyl)methylamino}methoxyboryl)oxide

: 142039-17-6
1,2-bis({(2,6-diisopropylphenyl)methylamino}methoxyboryl)ethyne

Guidance literature:: With Na/K; naphthalene; In 1,2-dimethoxyethane; byproducts: 1',2',3,3',4,4'-hexahydro-1,2'-binaphthyl; N2 atmosphere; addn. of naphthalene to suspn. of Na/K alloy in DME with stirring, stirring (6 h), addn. of B-compd., refluxing (6 h); removal of solvent (vac.), distn.; elem. anal.;