6-Methoxyharman

Base Information

Chemical Name:6-Methoxyharman
CAS No.:3589-72-8
Molecular Formula:C13H12N2O
Molecular Weight:212.25
Hs Code.:2933990090
NSC Number:92536
UNII:48GQI7H930
DSSTox Substance ID:DTXSID40189449
Nikkaji Number:J412.246A
Wikipedia:Isoharmine
Wikidata:Q15426262
Metabolomics Workbench ID:130010
ChEMBL ID:CHEMBL278193
Mol file:3589-72-8.mol

Synonyms:6-Methoxyharman;3589-72-8;Isoharmine;6-methoxy-1-methyl-9H-pyrido[3,4-b]indole;6-Methoxyharmane;Coharmine;6-Methoxy-1-methyl-9H-pyrido(3,4-b)indole;9H-Pyrido(3,4-b)indole, 6-methoxy-1-methyl-;6-Methoxy Harman;9H-Pyrido[3,4-b]indole,6-methoxy-1-methyl-;NSC 92536;BRN 0178687;CHEMBL278193;48GQI7H930;NSC-92536;4-23-00-02701 (Beilstein Handbook Reference);NSC92536;Oprea1_024115;UNII-48GQI7H930;SCHEMBL5035404;DTXSID40189449;XYYVPBBISSKKQB-UHFFFAOYSA-N;BDBM50132122;AKOS037651093;6-Methoxy-1-methyl-9H-beta-carboline;.beta.-Carboline, 6-methoxy-1-methyl-;6-Methoxy-1-methyl-9H-beta-carboline #;CS-15875;LS-133547;CS-0062557;D72284;Q15426262

Suppliers and Price of 6-Methoxyharman

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemenu
6-Methoxy-1-methyl-9H-pyrido[3,4-b]indole 95%+
1g
$ 2500.00

Chemenu
6-Methoxy-1-methyl-9H-pyrido[3,4-b]indole 95%+
250mg
$ 985.00

Chemenu
6-Methoxy-1-methyl-9H-pyrido[3,4-b]indole 95%+
100mg
$ 682.00

American Custom Chemicals Corporation
6-METHOXYHARMAN 95.00%
5MG
$ 498.10

AccelPharmtech
6-methoxy-1-methyl-9H-Pyrido[3,4-b]indole 97.00%
25G
$ 7320.00

AccelPharmtech
6-methoxy-1-methyl-9H-Pyrido[3,4-b]indole 97.00%
5G
$ 3900.00

Total 11 raw suppliers

Chemical Property of 6-Methoxyharman

Chemical Property:

Vapor Pressure:6.42E-07mmHg at 25°C
Melting Point:275 °C
Refractive Index:1.706
Boiling Point:421.4 °C at 760 mmHg
PKA:15.57±0.40(Predicted)
Flash Point:139.7 °C
PSA：37.91000
Density:1.252 g/cm³
LogP:3.03310
Storage Temp.:2-8°C
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:212.094963011
Heavy Atom Count:16
Complexity:258

Purity/Quality:

99% ^*data from raw suppliers

6-Methoxy-1-methyl-9H-pyrido[3,4-b]indole 95%+ ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC=CC2=C1NC3=C2C=C(C=C3)OC
Description A further constituent of the stems and leaves of Virola cuspidata, this alkaloid is the fully unsaturated carboline corresponding to the preceding base. The ultraviolet spectrum in EtOH has absorption maxima at 232, 290, 296 and 354 mJ.1 with shoulders at 246, 257 and 285 mJ.1.

Technology Process of 6-Methoxyharman

There total 16 articles about 6-Methoxyharman which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 6-methoxy-1-methyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole trifluoroacetate

: 3589-72-8
6-methoxyharman

Guidance literature:: With 2 mol-% Pd/C; lithium carbonate; In ethanol; at 150 ℃; for 0.166667h; Sealed tube; Microwave irradiation;
DOI:10.1002/ejoc.201301580

Reference yield: 40.0%

: 1210-56-6
6-methoxy-1-methyl-1,2,3,4-tetrahydro-β-carboline

: 3589-72-8
6-methoxyharman

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; for 3h; Heating;
DOI:10.3987/COM-98-8399

Reference yield: 15.0%

: 73-31-4
5-methoxy-N-acetyl-tryptamine

: 3589-72-8
6-methoxyharman

Guidance literature:: 5-methoxy-N-acetyl-tryptamine; With trifluoromethylsulfonic anhydride; Triphenylphosphine oxide; In chlorobenzene; at 20 - 130 ℃; for 2h;

With manganese(IV) oxide; In chlorobenzene; at 130 ℃; for 4h;
DOI:10.1016/j.tet.2016.08.014