Cinnamaldehyde, (2,4-dinitrophenyl)hydrazone

Base Information

• Chemical Name: Cinnamaldehyde, (2,4-dinitrophenyl)hydrazone
• CAS No.: 20710-28-5
• Molecular Formula: C15H12 N4 O4
• Molecular Weight: 312.285
• NSC Number: 99808

Synonyms:Cinnamaldehyde, (2,4-dinitrophenyl)hydrazone;2-Propenal, 3-phenyl-, (2,4-dinitrophenyl)hydrazone;(2E)-1-(2,4-dinitrophenyl)-2-[(2E)-3-phenylprop-2-en-1-ylidene]hydrazine;NSC99808;CINNAMALDEHYDE(2,4-DINITROPHENYL)HYDRAZONE;RLSRMSQNTNYDMC-LVVPDBGKSA-N;NSC-99808;STK796648;AKOS001713542;SR-01000116259;SR-01000116259-1;(1E,2E)-3-Phenyl-2-propenal (2,4-dinitrophenyl)hydrazone #;2,4-dinitro-N-[(E)-[(E)-3-phenylprop-2-enylidene]amino]aniline;20710-28-5

Chemical Property of Cinnamaldehyde, (2,4-dinitrophenyl)hydrazone

Chemical Property:

• Vapor Pressure: 2.94E-10mmHg at 25°C
• Boiling Point: 503.3°Cat760mmHg
• Flash Point: 258.2°C
• Density: 1.31g/cm³
• XLogP3: 2.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 4
• Exact Mass: 312.08585488
• Heavy Atom Count: 23
• Complexity: 463

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C=CC=NNC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-]
• Isomeric SMILES: C1=CC=C(C=C1)/C=C/C=N/NC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of Cinnamaldehyde, (2,4-dinitrophenyl)hydrazone

There total 3 articles about Cinnamaldehyde, (2,4-dinitrophenyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(E)-3-phenylpropenal (14371-10-9) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → 1-(2,4-dinitrophenyl)-2-((E)-3-phenylallylidene)hydrazine (20710-28-5)

Guidance literature:

In ethanol; at 20 ℃; for 12h;

DOI:10.1016/j.ica.2019.05.030

Reference yield:

3-phenyl-propenal (104-55-2) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → 1-(2,4-dinitrophenyl)-2-((E)-3-phenylallylidene)hydrazine (20710-28-5)

Guidance literature:

DOI:10.1080/00397910600775309

Reference yield:

→ 1-(2,4-dinitrophenyl)-2-((E)-3-phenylallylidene)hydrazine (20710-28-5)

Guidance literature:

Di-trans-cinnamyliden-hydrazin, 1-Fluor-2,4-dinitro-benzol, EtOH, Δ;

upstream raw materials:

3-phenyl-propenal

(2,4-dinitro-phenyl)-hydrazine

(E)-3-phenylpropenal

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