Technology Process of Benzene, 1,4-bis(3,3-dimethoxy-1-propenyl)-2,5-dimethoxy-, (E,E)-
There total 1 articles about Benzene, 1,4-bis(3,3-dimethoxy-1-propenyl)-2,5-dimethoxy-, (E,E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
palladium diacetate; tris-(o-tolyl)phosphine;
at 110 ℃;
for 60h;
- Guidance literature:
-
With
hydrogenchloride;
In
acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 91 percent / 2 N hydrochloric acid / acetone
2: 1.) sodium methanolate / 1.) methanol, 70 deg C, 30 min, 2.) tetrahydrofuran, 70 deg C, 2 h
3: 94 percent / hydrogen / 10 percent Pd/C / ethyl acetate; methanol / 3 h / 80 °C
4: 92 percent / lithium aluminium hydride / tetrahydrofuran / 3 h / Heating
5: 90 percent / pyridinium chlorochromate, Celite, magnesium sulfate / CH2Cl2 / 3 h / 20 °C
With
hydrogenchloride; lithium aluminium tetrahydride; Celite; hydrogen; sodium methylate; magnesium sulfate; pyridinium chlorochromate;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetone;
