1,2,3,4,7,7-Hexachlorobicyclo[2.2.1]hept-2-ene

Base Information

• Chemical Name: 1,2,3,4,7,7-Hexachlorobicyclo[2.2.1]hept-2-ene
• CAS No.: 22039-38-9
• Molecular Formula: C₇H₄Cl₆
• Molecular Weight: 300.827
• NSC Number: 143933
• DSSTox Substance ID: DTXSID50944642
• Nikkaji Number: J1.610.243A
• Mol file: 22039-38-9.mol

Synonyms:22039-38-9;1,2,3,4,7,7-hexachlorobicyclo[2.2.1]hept-2-ene;NSC143933;SCHEMBL3785870;DTXSID50944642;1,2,3,4,7,7-hexachloronorbornene;NSC 143933;NSC-143933;1,2,3,4,7,7-Hexachlorobicyclo[2.2.1]hepta-2-ene;Bicyclo(2.2.1)hept-2-ene, 1,2,3,4,7,7-hexachloro-

Chemical Property of 1,2,3,4,7,7-Hexachlorobicyclo[2.2.1]hept-2-ene

Chemical Property:

• Vapor Pressure: 0.00206mmHg at 25°C
• Boiling Point: 300°Cat760mmHg
• Flash Point: 135.8°C
• Density: 1.76g/cm³
• XLogP3: 3.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 299.841466
• Heavy Atom Count: 13
• Complexity: 280

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC2(C(=C(C1(C2(Cl)Cl)Cl)Cl)Cl)Cl

Technology Process of 1,2,3,4,7,7-Hexachlorobicyclo[2.2.1]hept-2-ene

There total 3 articles about 1,2,3,4,7,7-Hexachlorobicyclo[2.2.1]hept-2-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethene (74-85-1) + hexachlorocyclopentadiene (77-47-4) → 1,2,3,4,7,7-hexachlorobicyclo<2.2.1>hept-2-ene (22039-38-9)

Guidance literature:

at 210 ℃;

Reference yield:

1,2,3,4,7,7-hexachlorobicyclo[2.2.1]hepta-2,5-diene (3389-71-7) → 1,2,3,4,7,7-Hexachlor-bicyclo<2.2.1>hepten-(2) (22039-38-9)

Guidance literature:

Multistep reaction; (i) H₂, Pd-CaCO₃, EtOH, (ii) KOH;

DOI:10.1039/jr9620000457

Reference yield:

→ 1,2,3,4,7,7-Hexachlor-bicyclo<2.2.1>hepten-(2) (22039-38-9)

Guidance literature:

1,2,3,4,7,7-Hexachlor-bicyclo<2.2.1>hexa-2,5-dien, Hydrierung an Pt, Essigester;

DOI:10.1021/jo01031a024

upstream raw materials:

1,2,3,4,7,7-hexachlorobicyclo[2.2.1]hepta-2,5-diene

ethene

hexachlorocyclopentadiene

Downstream raw materials:

1,2,3,4,7-syn-Pentachlor-norbornen-(2)

1.4.7-Trichlor-norbornan