1H-Indene, 2-phenyl-1-(phenylmethylene)-, (E)-

Base Information

Chemical Name:1H-Indene, 2-phenyl-1-(phenylmethylene)-, (E)-
CAS No.:14272-88-9
Molecular Formula:C22H16
Molecular Weight:280.369
Hs Code.:

Synonyms:

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Chemical Property of 1H-Indene, 2-phenyl-1-(phenylmethylene)-, (E)-

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Technology Process of 1H-Indene, 2-phenyl-1-(phenylmethylene)-, (E)-

There total 13 articles about 1H-Indene, 2-phenyl-1-(phenylmethylene)-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1229445-69-5
(E)-1-(2,2-dibromovinyl)-2-styrylbenzene

: 98-80-6
phenylboronic acid

: 14272-88-9
(E)-2-phenyl-1-(phenylmethylene)-1H-indene

Guidance literature:: (E)-1-(2,2-dibromovinyl)-2-styrylbenzene; phenylboronic acid; With caesium carbonate; In 1,4-dioxane; water; Inert atmosphere;

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; In 1,4-dioxane; water; at 60 ℃; Inert atmosphere;
DOI:10.1021/ol100844v

Reference yield: 67.0%

: 13203-60-6
1,2-bis(2-phenylethynyl)benzene

: 14272-88-9
(E)-2-phenyl-1-(phenylmethylene)-1H-indene

Guidance literature:: 1,2-bis(2-phenylethynyl)benzene; With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 2h; Inert atmosphere; Reflux;

With hydrogenchloride; In dichloromethane; water; Reagent/catalyst; Solvent; Inert atmosphere;
DOI:10.1021/jacs.6b08540

Reference yield:

: 536-74-3
phenylacetylene

: 14272-88-9
(E)-2-phenyl-1-(phenylmethylene)-1H-indene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 77 percent / CuI; Et₃N / bis(triphenylphosphine)palladium(II) dichloride / Heating

2.1: Bu₃SnH; AIBN / toluene / 2 h / Heating

2.2: aq. HCl / CH₂Cl₂ / 1 h

With copper(l) iodide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In toluene; 1.1: Sonogashira coupling;
DOI:10.1039/b417493n