2-Propenoic acid, 3-[5-(1-methylcyclohexyl)-2-[7-(1-methylcyclohexyl)naphtho[2,1-b]furan-2 -yl]phenyl]-, 2,3-dichloro-5,6-dicyano-1,4-phenylene ester, (Z,Z)-

Base Information

• Chemical Name: 2-Propenoic acid, 3-[5-(1-methylcyclohexyl)-2-[7-(1-methylcyclohexyl)naphtho[2,1-b]furan-2 -yl]phenyl]-, 2,3-dichloro-5,6-dicyano-1,4-phenylene ester, (Z,Z)-
• CAS No.: 142834-85-3
• Molecular Formula: C78H74Cl2N2O6
• Molecular Weight: 1206.36

Synonyms:

Chemical Property of 2-Propenoic acid, 3-[5-(1-methylcyclohexyl)-2-[7-(1-methylcyclohexyl)naphtho[2,1-b]furan-2 -yl]phenyl]-, 2,3-dichloro-5,6-dicyano-1,4-phenylene ester, (Z,Z)-

Chemical Property:

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Technology Process of 2-Propenoic acid, 3-[5-(1-methylcyclohexyl)-2-[7-(1-methylcyclohexyl)naphtho[2,1-b]furan-2 -yl]phenyl]-, 2,3-dichloro-5,6-dicyano-1,4-phenylene ester, (Z,Z)-

There total 2 articles about 2-Propenoic acid, 3-[5-(1-methylcyclohexyl)-2-[7-(1-methylcyclohexyl)naphtho[2,1-b]furan-2 -yl]phenyl]-, 2,3-dichloro-5,6-dicyano-1,4-phenylene ester, (Z,Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.6%

6,7'-di(1-methylcyclohexyl)-spiro(naphthalene-1(2H),2'(1'H)-naphtho<2,1-b>furan)-2-one (115755-56-1) + 2,3-dicyano-5,6-dichloro-p-benzoquinone (84-58-2) → C35H36O2 (143210-06-4) + C78H74Cl2N2O6 (142834-85-3)

Guidance literature:

In benzene; for 24h; Heating;

DOI:10.1016/S0040-4020(01)88302-2

Reference yield:

6,7'-di(1-methylcyclohexyl)-spiro(naphthalene-1(2H),2'(1'H)-naphtho<2,1-b>furan)-2-one (115755-56-1) + 2,3-dicyano-5,6-dichloro-p-benzoquinone (84-58-2) → C78H74Cl2N2O6 (142834-85-3)

Guidance literature:

In benzene; Heating;

DOI:10.1016/S0040-4020(01)80451-8

Reference yield: 81.0%

C78H74Cl2N2O6 (142834-85-3) → (Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-prop-2-en-1-ol (142834-78-4)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; 1) 0 deg C, 2 h, 2) rt, 2 h;

DOI:10.1016/S0040-4020(01)80451-8

upstream raw materials:

6,7'-di(1-methylcyclohexyl)-spiro(naphthalene-1(2H),2'(1'H)-naphtho<2,1-b>furan)-2-one

2,3-dicyano-5,6-dichloro-p-benzoquinone

Downstream raw materials:

(Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-acrylic acid 2,3-dichloro-5,6-dicyano-4-methoxy-phenyl ester

(Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-prop-2-en-1-ol

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