(Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-acrylic acid 2,3-dichloro-5,6-dicyano-4-methoxy-phenyl ester

Base Information

• Chemical Name: (Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-acrylic acid 2,3-dichloro-5,6-dicyano-4-methoxy-phenyl ester
• CAS No.: 142834-87-5
• Molecular Formula: C₄₄H₄₀Cl₂N₂O₄
• Molecular Weight: 731.719

Synonyms:

Chemical Property of (Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-acrylic acid 2,3-dichloro-5,6-dicyano-4-methoxy-phenyl ester

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Technology Process of (Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-acrylic acid 2,3-dichloro-5,6-dicyano-4-methoxy-phenyl ester

There total 1 articles about (Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-acrylic acid 2,3-dichloro-5,6-dicyano-4-methoxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + methanol (67-56-1) + C78H74Cl2N2O6 (142834-85-3) → (Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-acrylic acid methyl ester + (Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-acrylic acid 2,3-dichloro-5,6-dicyano-4-methoxy-phenyl ester (142834-87-5)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given; 1) reflux, 3 days, 2) Et₂O, 0 deg C, 5 min;

DOI:10.1016/S0040-4020(01)80451-8

Reference yield: 40.0%

(Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-acrylic acid 2,3-dichloro-5,6-dicyano-4-methoxy-phenyl ester (142834-87-5) → (Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-prop-2-en-1-ol (142834-78-4)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; 1) 0 deg C, 2 h, 2) rt, 2 h;

DOI:10.1016/S0040-4020(01)80451-8

upstream raw materials:

diazomethane

methanol

C₇₈H₇₄Cl₂N₂O₆

Downstream raw materials:

(Z)-3-{5-(1-Methyl-cyclohexyl)-2-[7-(1-methyl-cyclohexyl)-naphtho[2,1-b]furan-2-yl]-phenyl}-prop-2-en-1-ol

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