Propanamide, N-phenyl-N-(2-(tetrahydro-3-(1-methylethyl)-1(2H)-pyrimidinyl)ethyl)-, ethanedioate, hydrate (2:4:1)

Base Information

Chemical Name:Propanamide, N-phenyl-N-(2-(tetrahydro-3-(1-methylethyl)-1(2H)-pyrimidinyl)ethyl)-, ethanedioate, hydrate (2:4:1)
CAS No.:77869-75-1
Molecular Formula:2C₂H₂O₄*C₁₈H₂₉N₃O
Molecular Weight:483.519
Hs Code.:
DSSTox Substance ID:DTXSID60228485

Synonyms:N-(2-(3-Isopropylhexahydropyrimidino)ethyl)propionanilide oxalate hydrate;Propanamide, N-phenyl-N-(2-(tetrahydro-3-(1-methylethyl)-1(2H)-pyrimidinyl)ethyl)-, ethanedioate, hydrate (2:4:1);77869-75-1;DTXSID60228485;LS-119375;C18H29N3O.2C2H2O4.1/2H2O;C18-H29-N3-O.2C2-H2-O4.1/2H2-O

Suppliers and Price of Propanamide, N-phenyl-N-(2-(tetrahydro-3-(1-methylethyl)-1(2H)-pyrimidinyl)ethyl)-, ethanedioate, hydrate (2:4:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Propanamide, N-phenyl-N-(2-(tetrahydro-3-(1-methylethyl)-1(2H)-pyrimidinyl)ethyl)-, ethanedioate, hydrate (2:4:1)

Chemical Property:

Vapor Pressure:4.07E-07mmHg at 25°C
Boiling Point:415.6°Cat760mmHg
Flash Point:160.6°C
PSA：175.99000
Density:g/cm³
LogP:0.99020
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:11
Rotatable Bond Count:8
Exact Mass:483.22167964
Heavy Atom Count:34
Complexity:411

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCC(=O)N(CCN1CCCN(C1)C(C)C)C2=CC=CC=C2.C(=O)(C(=O)O)O.C(=O)(C(=O)O)O

Technology Process of Propanamide, N-phenyl-N-(2-(tetrahydro-3-(1-methylethyl)-1(2H)-pyrimidinyl)ethyl)-, ethanedioate, hydrate (2:4:1)

There total 4 articles about Propanamide, N-phenyl-N-(2-(tetrahydro-3-(1-methylethyl)-1(2H)-pyrimidinyl)ethyl)-, ethanedioate, hydrate (2:4:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.1%

: 144-62-7,97993-78-7
oxalic acid

: 77869-74-0
N-<2-(3-isopropylhexahydropyrimidino)ethyl>propionanilide

: 77869-75-1
N-[2-(3-Isopropyl-tetrahydro-pyrimidin-1-yl)-ethyl]-N-phenyl-propionamide; compound with oxalic acid

Guidance literature:: In diethyl ether;
DOI:10.1248/cpb.28.3310

Reference yield:

: 77869-55-7
1-isopropylhexahydropyrimidine

: 77869-75-1
N-[2-(3-Isopropyl-tetrahydro-pyrimidin-1-yl)-ethyl]-N-phenyl-propionamide; compound with oxalic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 87.6 percent / ethanol / 4 h / Heating

2: benzene / 3 h / Heating

3: 21.1 percent / diethyl ether

In diethyl ether; ethanol; benzene;
DOI:10.1248/cpb.28.3310

Reference yield:

: 1005-66-9
N-(β-bromoethyl)aniline hydrobromide

: 77869-75-1
N-[2-(3-Isopropyl-tetrahydro-pyrimidin-1-yl)-ethyl]-N-phenyl-propionamide; compound with oxalic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 87.6 percent / ethanol / 4 h / Heating

2: benzene / 3 h / Heating

3: 21.1 percent / diethyl ether

In diethyl ether; ethanol; benzene;
DOI:10.1248/cpb.28.3310