tert-Butyl (diphenylmethyl)ethenylcarbamate

Base Information

Chemical Name:tert-Butyl (diphenylmethyl)ethenylcarbamate
CAS No.:142977-36-4
Molecular Formula:C₂₀H₂₃NO₂
Molecular Weight:309.408
Hs Code.:
DSSTox Substance ID:DTXSID80565405
Wikidata:Q82450481

Synonyms:tert-Butyl (diphenylmethyl)ethenylcarbamate;142977-36-4;DTXSID80565405

Suppliers and Price of tert-Butyl (diphenylmethyl)ethenylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of tert-Butyl (diphenylmethyl)ethenylcarbamate

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:309.172878976
Heavy Atom Count:23
Complexity:369

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)N(C=C)C(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of tert-Butyl (diphenylmethyl)ethenylcarbamate

There total 4 articles about tert-Butyl (diphenylmethyl)ethenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 142977-30-8
N-diphenylmethyl-N-vinylcarbamoyl chloride

: 75-65-0
tert-butyl alcohol

: 142977-36-4
t-butyl N-diphenylmethyl-N-vinylcarbamate

Guidance literature:: With sodium hydride; In tetrahydrofuran; 0 deg C -> r.t.;
DOI:10.1016/S0040-4039(00)92669-8

Reference yield:

: 91-00-9
Benzhydrylamine

: 142977-36-4
t-butyl N-diphenylmethyl-N-vinylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: MgSO₄ / diethyl ether / 12 h / 0 °C

2: Et₃N / benzene / 3 h / Ambient temperature

3: Heating

4: 28 percent / 60 percent NaH / tetrahydrofuran; paraffin

With sodium hydride; magnesium sulfate; triethylamine; In tetrahydrofuran; diethyl ether; paraffin; benzene;
DOI:10.1016/S0040-4020(01)89665-4

Reference yield:

: 169698-45-7
N-(diphenylmethyl)ethanimine

: 142977-36-4
t-butyl N-diphenylmethyl-N-vinylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / benzene / 3 h / Ambient temperature

2: Heating

3: 28 percent / 60 percent NaH / tetrahydrofuran; paraffin

With sodium hydride; triethylamine; In tetrahydrofuran; paraffin; benzene;
DOI:10.1016/S0040-4020(01)89665-4