Benzene, 1-methoxy-4-methyl-2-(2-propynyloxy)-

Base Information

Chemical Name:Benzene, 1-methoxy-4-methyl-2-(2-propynyloxy)-
CAS No.:143261-00-1
Molecular Formula:C11H12O2
Molecular Weight:176.215
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-methoxy-4-methyl-2-(2-propynyloxy)-

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Technology Process of Benzene, 1-methoxy-4-methyl-2-(2-propynyloxy)-

There total 1 articles about Benzene, 1-methoxy-4-methyl-2-(2-propynyloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.3%

: 1195-09-1
5-methyl-2-methoxyphenol

: 106-96-7
propargyl bromide

: 143261-00-1
4-methoxy-3-(2-propynyloxy)toluene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 5h; Ambient temperature;
DOI:10.1248/cpb.40.1148

Reference yield:

: 143261-00-1
4-methoxy-3-(2-propynyloxy)toluene

: 16273-16-8
2,3-dimethoxy-6-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 80.2 percent / CsF, PhNEt₂ / 8 h / Heating

2: 1.) OsO₄, pyridine, 2.) sodium hydrogen sulfite / 1.) RT, 4 h, 2.) water, RT, 1.5 h

3: 83.7 percent / sodium metaperiodate / methanol; H₂O / 5 h / Ambient temperature

4: 100 percent / sodium hydroxide, benzyl tri-n-butylammonium chloride / CH₂Cl₂; H₂O / 1.5 h / Ambient temperature

With pyridine; sodium hydroxide; sodium periodate; osmium(VIII) oxide; benzyltri(n-butyl)ammonium chloride; sodium hydrogensulfite; cesium fluoride; N,N-diethylaniline; In methanol; dichloromethane; water;
DOI:10.1248/cpb.40.1148

Reference yield:

: 143261-00-1
4-methoxy-3-(2-propynyloxy)toluene

: 143261-05-6
2-hydroxy-3-methoxy-6-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 80.2 percent / CsF, PhNEt₂ / 8 h / Heating

2: 1.) OsO₄, pyridine, 2.) sodium hydrogen sulfite / 1.) RT, 4 h, 2.) water, RT, 1.5 h

3: 83.7 percent / sodium metaperiodate / methanol; H₂O / 5 h / Ambient temperature

With pyridine; sodium periodate; osmium(VIII) oxide; sodium hydrogensulfite; cesium fluoride; N,N-diethylaniline; In methanol; water;
DOI:10.1248/cpb.40.1148