1,3,5-Triazine-1(2H)-hexanoic acid, a-[[(1,1-dimethylethoxy)carbonyl]amino]tetrahydro-4-oxo-3,5-bis(phenyl methyl)-, methyl ester, (S)-

Base Information

Chemical Name:1,3,5-Triazine-1(2H)-hexanoic acid, a-[[(1,1-dimethylethoxy)carbonyl]amino]tetrahydro-4-oxo-3,5-bis(phenyl methyl)-, methyl ester, (S)-
CAS No.:143565-39-3
Molecular Formula:C₂₉H₄₀N₄O₅
Molecular Weight:524.66
Hs Code.:

Synonyms:

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Chemical Property of 1,3,5-Triazine-1(2H)-hexanoic acid, a-[[(1,1-dimethylethoxy)carbonyl]amino]tetrahydro-4-oxo-3,5-bis(phenyl methyl)-, methyl ester, (S)-

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Technology Process of 1,3,5-Triazine-1(2H)-hexanoic acid, a-[[(1,1-dimethylethoxy)carbonyl]amino]tetrahydro-4-oxo-3,5-bis(phenyl methyl)-, methyl ester, (S)-

There total 4 articles about 1,3,5-Triazine-1(2H)-hexanoic acid, a-[[(1,1-dimethylethoxy)carbonyl]amino]tetrahydro-4-oxo-3,5-bis(phenyl methyl)-, methyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73548-77-3
Boc-L-Lys(Z)-OMe

: 143565-39-3
methyl 2(S)-<(tert-butoxycarbonyl)amino>-6-(1,3-dibenzylhexahydro-2-oxo-1,3,5-triazin-5-yl)hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd-C / methanol / 0.75 h / 760 Torr

2: 1) i-Pr₂NEt / 1) H₂O, 10 min, 2) EtOAc, reflux, 20 h

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00049a036

Reference yield:

: 3173-56-6
benzyl isothiocyanate

: 143565-39-3
methyl 2(S)-<(tert-butoxycarbonyl)amino>-6-(1,3-dibenzylhexahydro-2-oxo-1,3,5-triazin-5-yl)hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / CH₂Cl₂ / 0.5 h / 5 °C

2: 1) i-Pr₂NEt / 1) H₂O, 10 min, 2) EtOAc, reflux, 20 h

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo00049a036

Reference yield:

: 100-46-9
benzylamine

: 143565-39-3
methyl 2(S)-<(tert-butoxycarbonyl)amino>-6-(1,3-dibenzylhexahydro-2-oxo-1,3,5-triazin-5-yl)hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / CH₂Cl₂ / 0.5 h / 5 °C

2: 1) i-Pr₂NEt / 1) H₂O, 10 min, 2) EtOAc, reflux, 20 h

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo00049a036