Technology Process of 5-Hydroxy-1-(4-hydroxy-3-methoxyphenyl)-3-pentanone
There total 7 articles about 5-Hydroxy-1-(4-hydroxy-3-methoxyphenyl)-3-pentanone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen fluoride;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrogen / 5percent palladium on carbon / methanol
2: 78 percent / diethyl phosphorocyanidate, triethylamine / dimethylformamide
3: 89 percent / p-toluenesulfonic acid / benzene / Heating
4: 76 percent / diisobutylaluminum hydride / diethyl ether / 1 h / -20 °C
5: 84 percent / sodium borohydride
6: 68 percent / hydrogen fluoride
With
sodium tetrahydroborate; diethyl cyanophosphonate; hydrogen fluoride; hydrogen; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine;
palladium on activated charcoal;
In
methanol; diethyl ether; N,N-dimethyl-formamide; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 78 percent / diethyl phosphorocyanidate, triethylamine / dimethylformamide
2: 89 percent / p-toluenesulfonic acid / benzene / Heating
3: 76 percent / diisobutylaluminum hydride / diethyl ether / 1 h / -20 °C
4: 84 percent / sodium borohydride
5: 68 percent / hydrogen fluoride
With
sodium tetrahydroborate; diethyl cyanophosphonate; hydrogen fluoride; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine;
In
diethyl ether; N,N-dimethyl-formamide; benzene;