1-Hexanol, 6-(phenylmethoxy)-2-(2-propenyl)-, (R)-

Base Information

Chemical Name:1-Hexanol, 6-(phenylmethoxy)-2-(2-propenyl)-, (R)-
CAS No.:143761-25-5
Molecular Formula:C16H24O2
Molecular Weight:248.365
Hs Code.:

Synonyms:

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Chemical Property of 1-Hexanol, 6-(phenylmethoxy)-2-(2-propenyl)-, (R)-

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Technology Process of 1-Hexanol, 6-(phenylmethoxy)-2-(2-propenyl)-, (R)-

There total 5 articles about 1-Hexanol, 6-(phenylmethoxy)-2-(2-propenyl)-, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 143761-24-4
(2'R,4S)-4-benzyl-3-<2'-allyl-6'-(benzyloxy)hexanoyl>oxazolidin-2-one

: 143761-25-5
2(R)-allyl-6-(benzyloxy)hexan-1-ol

Guidance literature:: With lithium borohydride; water; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 0.5h;
DOI:10.1021/jm00054a003

Reference yield:

: 130892-97-6
6-benzyloxyhexanoic acid

: 143761-25-5
2(R)-allyl-6-(benzyloxy)hexan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / diethyl ether / 2 h / 0 °C

2: 1.) n-BuLi / 1.) THF, hexane, 2.) THF, from -78 deg to RT, 1 h

3: 1.) LDA / 1) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, -10 deg C, 2 h

4: 83 percent / LiBH₄, H₂O / diethyl ether; tetrahydrofuran / 0.5 h / 0 - 20 °C

With lithium borohydride; n-butyllithium; water; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jm00054a003

Reference yield:

: C₁₈H₂₆O₄

: 143761-25-5
2(R)-allyl-6-(benzyloxy)hexan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, hexane, 2.) THF, from -78 deg to RT, 1 h

2: 1.) LDA / 1) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, -10 deg C, 2 h

3: 83 percent / LiBH₄, H₂O / diethyl ether; tetrahydrofuran / 0.5 h / 0 - 20 °C

With lithium borohydride; n-butyllithium; water; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jm00054a003