Octanoic acid, 8-(phenylmethoxy)-4-(2-propenyl)-, methyl ester, (S)-

Base Information

Chemical Name:Octanoic acid, 8-(phenylmethoxy)-4-(2-propenyl)-, methyl ester, (S)-
CAS No.:143761-29-9
Molecular Formula:C19H28O3
Molecular Weight:304.43
Hs Code.:

Synonyms:

Suppliers and Price of Octanoic acid, 8-(phenylmethoxy)-4-(2-propenyl)-, methyl ester, (S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of Octanoic acid, 8-(phenylmethoxy)-4-(2-propenyl)-, methyl ester, (S)-

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Octanoic acid, 8-(phenylmethoxy)-4-(2-propenyl)-, methyl ester, (S)-

There total 8 articles about Octanoic acid, 8-(phenylmethoxy)-4-(2-propenyl)-, methyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₆O₄

: 143761-29-9
(4S)-methyl 4-allyl-8-(benzyloxy)octanoate

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) n-BuLi / 1.) THF, hexane, 2.) THF, from -78 deg to RT, 1 h

2: 1.) LDA / 1) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, -10 deg C, 2 h

3: 83 percent / LiBH₄, H₂O / diethyl ether; tetrahydrofuran / 0.5 h / 0 - 20 °C

4: 100 percent / Et₃N / CH₂Cl₂ / 2 h / 0 °C

5: 1.) NaH / 1.) THF, RT, 30 min, 2.) THF, reflux, 18 h

6: aq. KOH / dioxane / 18 h / Ambient temperature

7: 3 h / 125 - 140 °C

8: diethyl ether / 0.17 h / 0 °C

With potassium hydroxide; lithium borohydride; n-butyllithium; water; sodium hydride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane;
DOI:10.1021/jm00054a003

Reference yield:

: 143761-25-5
2(R)-allyl-6-(benzyloxy)hexan-1-ol

: 143761-29-9
(4S)-methyl 4-allyl-8-(benzyloxy)octanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / Et₃N / CH₂Cl₂ / 2 h / 0 °C

2: 1.) NaH / 1.) THF, RT, 30 min, 2.) THF, reflux, 18 h

3: aq. KOH / dioxane / 18 h / Ambient temperature

4: 3 h / 125 - 140 °C

5: diethyl ether / 0.17 h / 0 °C

With potassium hydroxide; sodium hydride; triethylamine; In 1,4-dioxane; diethyl ether; dichloromethane;
DOI:10.1021/jm00054a003

Reference yield:

: 143761-26-6
Methanesulfonic acid (R)-2-allyl-6-benzyloxy-hexyl ester

: 143761-29-9
(4S)-methyl 4-allyl-8-(benzyloxy)octanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) THF, RT, 30 min, 2.) THF, reflux, 18 h

2: aq. KOH / dioxane / 18 h / Ambient temperature

3: 3 h / 125 - 140 °C

4: diethyl ether / 0.17 h / 0 °C

With potassium hydroxide; sodium hydride; In 1,4-dioxane; diethyl ether;
DOI:10.1021/jm00054a003