2-Phenylnaphtho[1,2-B]furan

Base Information

• Chemical Name: 2-Phenylnaphtho[1,2-B]furan
• CAS No.: 14385-53-6
• Molecular Formula: C18H12O
• Molecular Weight: 244.293
• ChEMBL ID: CHEMBL3230199
• DSSTox Substance ID: DTXSID10505076
• Wikidata: Q82359938

Synonyms:2-PHENYLNAPHTHO[1,2-B]FURAN;14385-53-6;CHEMBL3230199;SCHEMBL11646604;DTXSID10505076

Chemical Property of 2-Phenylnaphtho[1,2-B]furan

Chemical Property:

• XLogP3: 5.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 244.088815002
• Heavy Atom Count: 19
• Complexity: 307

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=CC3=C(O2)C4=CC=CC=C4C=C3

Technology Process of 2-Phenylnaphtho[1,2-B]furan

There total 17 articles about 2-Phenylnaphtho[1,2-B]furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 3,4-dihydronaphthalene-1(2H)-one (529-34-0) → phenyl-2 naphto<1,2-b>furanne (14385-53-6)

Guidance literature:

With copper(II) acetate monohydrate; silver carbonate; tri tert-butylphosphoniumtetrafluoroborate; In 2,2,2-trifluoroethanol; at 130 ℃; for 24h; Solvent; Reagent/catalyst; Time; Concentration;

DOI:10.1002/anie.201609401

Reference yield: 89.0%

C18H16O3 → phenyl-2 naphto<1,2-b>furanne (14385-53-6)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; at 40 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tet.2017.11.049

Reference yield: 83.2%

C19H14O4 → phenyl-2 naphto<1,2-b>furanne (14385-53-6)

Guidance literature:

With sodium acetate; acetic anhydride; at 120 - 125 ℃; for 4h;

DOI:10.1080/14756366.2021.1940993

upstream raw materials:

1-(naphthalen-1-yl)-2-phenoxyethan-1-one

3-(methylthio)-2-phenylnaphtho[1,2-b]furan

α-naphthol

2,2-dibromostyrene

Downstream raw materials:

formyl-3 phenyl-2 naphto<1,2-b>furanne

acetyl-3 phenyl-2 naphto<1,2-b>furanne

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