decachloro-1,4-dihydronaphthalene

Base Information

• Chemical Name: decachloro-1,4-dihydronaphthalene
• CAS No.: 14396-29-3
• Molecular Formula: C10Cl10
• Molecular Weight: 474.64
• Mol file: 14396-29-3.mol

Synonyms:

Chemical Property of decachloro-1,4-dihydronaphthalene

Chemical Property:

• Vapor Pressure: 6.81E-08mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of decachloro-1,4-dihydronaphthalene

There total 6 articles about decachloro-1,4-dihydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

naphthalene (91-20-3,71998-51-1,72931-45-4) → decachloro-1,4-dihydronaphthalene (14396-29-3)

Guidance literature:

With aluminium trichloride; sulfuryl dichloride; sulfur monochloride; for 5h; Heating;

Reference yield: 45.0%

1,4-dihydronaphthalene (612-17-9) → decachloro-1,4-dihydronaphthalene (14396-29-3)

Guidance literature:

With disulfur dichloride; aluminium trichloride; sulfuryl dichloride; at 64 ℃; for 4h;

DOI:10.1021/j100127a006

Reference yield:

2-Methylnaphthalene (91-57-6,34468-07-0) → decachloro-1,4-dihydronaphthalene (14396-29-3) + 2-(trichloromethyl)heptachloronaphthalene (150986-19-9)

Guidance literature:

With chlorine; iron; In sulfuryl dichloride; at 64 ℃;

DOI:10.1021/ja00071a054

upstream raw materials:

naphthalene

1,4-dihydronaphthalene

1-Methylnaphthalene

2-Methylnaphthalene

Downstream raw materials:

1,2,3,4,6,7-hexachloronaphthalene

1,2,3,5,6,7-hexachloronaphthalene

tetrachloromethane

perchloroindene

Refernces

• 1、 Sun, Jing,Grützmacher, Hans-Fr.,Lifshitz, Chava. "Ion/molecule reactions of carbon cluster ions and acrylonitrile". . p. 8382 - 8388. Retrieved 2007/10/02.
• 2、 Garcia, R.,Riera, J.,Carilla, J.,Julia, L.,Molins, E.,Miravitlles, C.. "Extensive Chlorination of Methylnaphthalenes, Friedel-Crafts Alkylation of Pentachlorobenzene by Heptachloro(chloromethyl)naphthalenes, and Related Results". . p. 5712 - 5719. Retrieved 2007/10/02.