9,10-dimethoxy-1,2,3,4-tetrahydro-1,4-methanoanthracene

Base Information

• Chemical Name: 9,10-dimethoxy-1,2,3,4-tetrahydro-1,4-methanoanthracene
• CAS No.: 75102-19-1
• Molecular Formula: C₁₇H₁₈O₂
• Molecular Weight: 254.329
• Mol file: 75102-19-1.mol

Synonyms:1,2,3,4-Tetrahydro-1:4-methano-9,10-dimethoxyanthracene

Chemical Property of 9,10-dimethoxy-1,2,3,4-tetrahydro-1,4-methanoanthracene

Chemical Property:

• Vapor Pressure: 7.4E-06mmHg at 25°C
• Boiling Point: 387.3°Cat760mmHg
• Flash Point: 156.6°C
• PSA: 18.46000
• Density: 1.171g/cm³
• LogP: 4.22170

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 9,10-dimethoxy-1,2,3,4-tetrahydro-1,4-methanoanthracene

There total 2 articles about 9,10-dimethoxy-1,2,3,4-tetrahydro-1,4-methanoanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,4-dihydro-9,10-dimethoxy-1,4-methanoanthracene (52457-25-7) → 9,10-dimethoxy-1,4-methano-1,2,3,4-tetrahydroanthracene (75102-19-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 3h; under 1551.4 Torr;

DOI:10.1021/jo01312a019

Reference yield: 91.0%

1,4-Dihydro-1,4-methano-9,10-dimethoxyanthracene (52457-25-7) → 1,2,3,4-Tetrahydro-1,4-methano-9,10-dimethoxyanthracene (75102-19-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate;

DOI:10.1002/mrc.1260320310

upstream raw materials:

1,4-dihydro-9,10-dimethoxy-1,4-methanoanthracene

1,4-Dihydro-1,4-methano-9,10-dimethoxyanthracene

Refernces

• 1、 Jiwan, J. L. Habib,Soumillion, J. Ph.. "Photoinduced Charge Separation in Rigid Bichromophoric Compounds and Charge Transfer State Electron Transfer Reactivity". . p. 14223 - 14230. Retrieved 2007/10/02.