2,4,6-tri-tert-Butylnitrosobenzene

Base Information

Chemical Name:2,4,6-tri-tert-Butylnitrosobenzene
CAS No.:24973-59-9
Molecular Formula:C18H29 N O
Molecular Weight:275.434
Hs Code.:2904209090
European Community (EC) Number:246-553-3
NSC Number:677542
UNII:SZX3GP4GT9
DSSTox Substance ID:DTXSID40179688
Nikkaji Number:J286.436C
Wikidata:Q83050215
Mol file:24973-59-9.mol

Synonyms:2,4,6-tri-tert-Butylnitrosobenzene;24973-59-9;1,3,5-Tritert-butyl-2-nitrosobenzene;1,3,5-Tri-tert-butyl-2-nitrosobenzene;Benzene, 1,3,5-tris(1,1-dimethylethyl)-2-nitroso-;2,4,6-Tri-t-butyl-nitrosobenzene;1,3,5-Tri(tert-butyl)-2-nitrosobenzene;NSC677542;SZX3GP4GT9;EINECS 246-553-3;NSC 677542;NSC-677542;TTBNB;2-Nitroso-1,3,5-tri-tert-butylbenzene;UNII-SZX3GP4GT9;SCHEMBL104121;2,4,6-tri-t-butylnitrosobenzene;DTXSID40179688;ZAA97359;MFCD00008817;AKOS004120290;1,3,5-tritert-butyl-2-nitroso-benzene;Nitrosobenzene, 2,4,6-tri-tert-butyl-;AS-68087;FT-0745688;T1534;T72161;J-640237;1,3,5-TRIS(1,1-DIMETHYLETHYL)-2-NITROSOBENZENE;1,3,5-Tri-tert-butyl-2-nitrosobenzene, for ESR-spectroscopy, >98.0% (HPLC)

Suppliers and Price of 2,4,6-tri-tert-Butylnitrosobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,4,6-Tri-tert-butylnitrosobenzene
500mg
$ 925.00

TRC
2,4,6-Tri-tert-butylnitrosobenzene
250mg
$ 550.00

TCI Chemical
2,4,6-Tri-tert-butylnitrosobenzene >98.0%(GC)
100mg
$ 70.00

TCI Chemical
2,4,6-Tri-tert-butylnitrosobenzene >98.0%(GC)
1g
$ 493.00

American Custom Chemicals Corporation
2,4,6-TRI-TERT-BUTYLNITROSOBENZENE 95.00%
1G
$ 890.40

American Custom Chemicals Corporation
2,4,6-TRI-TERT-BUTYLNITROSOBENZENE 95.00%
100MG
$ 594.86

AK Scientific
2,4,6-Tri-tert-butylnitrosobenzene
100mg
$ 139.00

Total 12 raw suppliers

Chemical Property of 2,4,6-tri-tert-Butylnitrosobenzene

Chemical Property:

Vapor Pressure:0.000671mmHg at 25°C
Melting Point:168-173oC
Refractive Index:1.5000 (estimate)
Boiling Point:318.5oC at 760 mmHg
Flash Point:130.2oC
PSA：29.43000
Density:0.9g/cm3
LogP:5.97700
Storage Temp.:2-8°C
XLogP3:6.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:275.224914549
Heavy Atom Count:20
Complexity:316

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,4,6-Tri-tert-butylnitrosobenzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CC(C)(C)C1=CC(=C(C(=C1)C(C)(C)C)N=O)C(C)(C)C

Technology Process of 2,4,6-tri-tert-Butylnitrosobenzene

There total 7 articles about 2,4,6-tri-tert-Butylnitrosobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 961-38-6
2,4,6-Tri-tert-butylaniline

: 24973-59-9
2,4,6-tri-tert-butyl-1-nitrosobenzene

Guidance literature:: With C₁₉H₁₈N₆O₂*2Cl^(1-)*3H₂O*Mn⁽²⁺⁾; dihydrogen peroxide; In methanol; at 45 ℃; for 48h;
DOI:10.1016/j.ica.2010.06.064

Reference yield: 21.0%

: 961-38-6
2,4,6-Tri-tert-butylaniline

: 24973-59-9
2,4,6-tri-tert-butyl-1-nitrosobenzene

: 3383-21-9
3,5-di-tert-butyl-o-benzoquinone

: 4074-25-3
2,4,6-tri-tert-butylnitrobenzene

: 143726-74-3
2,4,6-tri-tert-butyl-4-tert-butylperoxy-2,5-cyclohexadien-1-imine

Guidance literature:: With (t-BuOO)Co(CH₂NCHC₆H₄O)2; In water; 1,2-dichloro-ethane; at 23 ℃; for 0.333333h; other reagents: 1.) PbO₂, 2.) tert-butyl hydroperoxide;
DOI:10.1021/jo952198p