2-Furancarboxylic acid, 5-[[[[(2-ethyl-6-methylphenyl)hydrazono][[(4-nitrophenyl)methyl]thio]meth yl]thio]methyl]-, methyl ester

Base Information

Chemical Name:2-Furancarboxylic acid, 5-[[[[(2-ethyl-6-methylphenyl)hydrazono][[(4-nitrophenyl)methyl]thio]meth yl]thio]methyl]-, methyl ester
CAS No.:144269-01-2
Molecular Formula:C₂₄H₂₅N₃O₅S₂
Molecular Weight:499.612
Hs Code.:
Mol file:144269-01-2.mol

Synonyms:

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Chemical Property of 2-Furancarboxylic acid, 5-[[[[(2-ethyl-6-methylphenyl)hydrazono][[(4-nitrophenyl)methyl]thio]meth yl]thio]methyl]-, methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 2-Furancarboxylic acid, 5-[[[[(2-ethyl-6-methylphenyl)hydrazono][[(4-nitrophenyl)methyl]thio]meth yl]thio]methyl]-, methyl ester

There total 3 articles about 2-Furancarboxylic acid, 5-[[[[(2-ethyl-6-methylphenyl)hydrazono][[(4-nitrophenyl)methyl]thio]meth yl]thio]methyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 144268-92-8
5-methoxycarbonyl-2-furfuryl-3-(2-ethyl-6-methyl)dithiocarbazate

: 144269-01-2
N-(2-ethyl-6-methylphenylamino)-S-(4-nitrobenzyl)-S-(5-methoxycarbonyl-2-furfuryl)imidodithiocarbonate

Guidance literature:: With potassium hydroxide; Yield given. Multistep reaction; 1.) MeOH, 15 deg C, 2.) MeOH, 25 deg C, 3 h;
DOI:10.1135/cccc19921699

Reference yield:

: 2144-37-8
methyl 5-(chloromethyl)-2-furoate

: 144269-01-2
N-(2-ethyl-6-methylphenylamino)-S-(4-nitrobenzyl)-S-(5-methoxycarbonyl-2-furfuryl)imidodithiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) conc. aq. NH₃ / 1.) EtOH, 25-30 deg C, 1 h, 2.) EtOH, 25-30 deg C, 24 h

2: 1.) KOH / 1.) MeOH, 15 deg C, 2.) MeOH, 25 deg C, 3 h

With potassium hydroxide; ammonium hydroxide;
DOI:10.1135/cccc19921699

Reference yield:

: 74404-34-5
2-ethyl-6-methylphenylhydrazine

: 144269-01-2
N-(2-ethyl-6-methylphenylamino)-S-(4-nitrobenzyl)-S-(5-methoxycarbonyl-2-furfuryl)imidodithiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) conc. aq. NH₃ / 1.) EtOH, 25-30 deg C, 1 h, 2.) EtOH, 25-30 deg C, 24 h

2: 1.) KOH / 1.) MeOH, 15 deg C, 2.) MeOH, 25 deg C, 3 h

With potassium hydroxide; ammonium hydroxide;
DOI:10.1135/cccc19921699