Bis(alpha-methoxy-p-tolyl) ether

Base Information

• Chemical Name: Bis(alpha-methoxy-p-tolyl) ether
• CAS No.: 2509-26-4
• Molecular Formula: C16H18O3
• Molecular Weight: 258.317
• Hs Code.: 2909309090
• European Community (EC) Number: 219-722-4
• UNII: KCF4ZXZ9P8
• DSSTox Substance ID: DTXSID90179779
• Nikkaji Number: J60.133K
• Wikidata: Q72446200
• Mol file: 2509-26-4.mol

Synonyms:2509-26-4;4,4'-Oxybis((methoxymethyl)benzene);4,4'-Bis(methoxymethyl)diphenyl ether;Bis(alpha-methoxy-p-tolyl) ether;1-(methoxymethyl)-4-[4-(methoxymethyl)phenoxy]benzene;Benzene, 1,1'-oxybis[4-(methoxymethyl)-;EINECS 219-722-4;KCF4ZXZ9P8;4,4'-Oxybis[(methoxymethyl)benzene];Ether, bis(.alpha.-methoxy-p-tolyl);Benzene, 1,1'-oxybis(4-(methoxymethyl)-;UNII-KCF4ZXZ9P8;SCHEMBL6327626;bis(4-methoxymethylphenyl) ether;DTXSID90179779;bis-(4-methoxymethylphenyl) ether;bis-(alpha-methoxy-p-tolyl) ether;4,4-Bismethoxymethyldiphenyl Ether;bis-(I+/--methoxy-p-tolyl) ether;MFCD00082840;4,4'-bis(methoxymethyl)diphenylether;AKOS016000699;Benzene,1,1'-oxybis[(methoxymethyl)-;AS-64063;CS-0210633;FT-0634334;O0537;1,1'-OXYBIS(4-(METHOXYMETHYL)BENZENE);D91884;A817638;1,1 inverted exclamation marka-Oxybis[4-(methoxymethyl)benzene]

Chemical Property of Bis(alpha-methoxy-p-tolyl) ether

Chemical Property:

• Vapor Pressure: 0.000217mmHg at 25°C
• Refractive Index: 1.544
• Boiling Point: 336.6 °C at 760 mmHg
• Flash Point: 113 °C
• PSA: 27.69000
• Density: 1.083 g/cm³
• LogP: 3.77170
• Storage Temp.: 2-8°C
• XLogP3: 2.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 258.125594432
• Heavy Atom Count: 19
• Complexity: 204

Purity/Quality:

98%,99%, ^*data from raw suppliers

4,4'-Oxybis[(methoxymethyl)benzene] ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COCC1=CC=C(C=C1)OC2=CC=C(C=C2)COC

Technology Process of Bis(alpha-methoxy-p-tolyl) ether

There total 3 articles about Bis(alpha-methoxy-p-tolyl) ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.8%

sodium methylate (124-41-4) + 1,1'-oxybis(4-methyl-benzene) (1579-40-4) → 4,4'-Bis-methoxymethyl diphenyl ether (2509-26-4)

Guidance literature:

1,1'-oxybis(4-methyl-benzene); With 2,2'-azobis(isobutyronitrile); bromine; In benzene; at 80 ℃; for 3h; Reflux;

sodium methylate; In methanol; at 45 ℃; for 2h; Temperature; Reflux;

Reference yield:

→ 4-azodiphenylamine + 4,4'-Bis-methoxymethyl diphenyl ether (2509-26-4)

Guidance literature:

Reference yield:

→ 4,4'-Bis-methoxymethyl diphenyl ether (2509-26-4)

Guidance literature:

4,4'-Bis-chlormethyl-diphenylether, KOH/MeOH;

upstream raw materials:

sodium methylate

1,1'-oxybis(4-methyl-benzene)

Refernces

• 1、 -. "Ionic halomethyl-1,3,5-triazine photoinitiators". . . Retrieved 2008/06/13.