Bicyclo[2.2.1]heptane-2-aceticacid, (1R,2S,4S)-rel-

Base Information

• Chemical Name: Bicyclo[2.2.1]heptane-2-aceticacid, (1R,2S,4S)-rel-
• CAS No.: 6485-19-4
• Molecular Formula: C₉H₁₄O₂
• Molecular Weight: 154.209

Synonyms:2-Norbornaneaceticacid, exo- (8CI); Bicyclo[2.2.1]heptane-2-acetic acid, exo-;exo-2-Norbornaneacetic acid; exo-2-Norbornylacetic acid

Chemical Property of Bicyclo[2.2.1]heptane-2-aceticacid, (1R,2S,4S)-rel-

Chemical Property:

• PSA: 37.30000
• LogP: 1.89730

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bicyclo[2.2.1]heptane-2-aceticacid, (1R,2S,4S)-rel-

There total 18 articles about Bicyclo[2.2.1]heptane-2-aceticacid, (1R,2S,4S)-rel- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

norborn-2-ene (498-66-8) + acetic anhydride (108-24-7) → bicyclo[2.2.1]heptan-2-ylacetic acid (6485-19-4,59331-96-3,1007-01-8)

Guidance literature:

With oxygen; cobalt(II) acetate; manganese(II) acetate; In acetic acid; at 130 ℃; for 5h;

DOI:10.1021/jo034584+

Reference yield: 5.0%

norborn-2-ene (498-66-8) + acetic acid (64-19-7,77671-22-8) → bicyclo[2.2.1]heptan-2-ylacetic acid (6485-19-4,59331-96-3,1007-01-8) + (3aα,4β,7β,7aα)-hexahydro-4,7-methanobenzofuran-2(3H)-one (5963-22-4,33045-15-7,54595-29-8,145632-53-7,693794-26-2) + ((1S,2R,3R,4R)-3-Acetoxy-bicyclo[2.2.1]hept-2-yl)-acetic acid (93863-20-8) + ((1S,2S,4S,7R)-2-Acetoxy-bicyclo[2.2.1]hept-7-yl)-acetic acid (93863-21-9,145576-08-5)

Guidance literature:

With potassium acetate; manganese triacetate; Further byproducts given; Heating;

DOI:10.1021/jo00201a003

Reference yield:

norborn-2-ene (498-66-8) + 1,1-Dichloroethylene (75-35-4,9002-85-1) → bicyclo[2.2.1]heptan-2-ylacetic acid (6485-19-4,59331-96-3,1007-01-8)

Guidance literature:

With sulfuric acid; boron trifluoride;

upstream raw materials:

(+/-)-2endo-chloromethyl-norbornane

endo-2-(bromomethyl)bicyclo<2.2.1>heptane

(+/-)-(norbornyl-(2endo))-acetonitrile

carbon dioxide

Downstream raw materials:

exo-Norbornyl-⁽²⁾-essigsaeure-anilid

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