Guanidine, N-[3-(5-methyl-1H-imidazol-4-yl)propyl]-N'-[2-[(phenylmethyl)thio]ethyl]-, compd. with 2,4,6-trinitrophenol (1:2)

Base Information

Chemical Name:Guanidine, N-[3-(5-methyl-1H-imidazol-4-yl)propyl]-N'-[2-[(phenylmethyl)thio]ethyl]-, compd. with 2,4,6-trinitrophenol (1:2)
CAS No.:144284-46-8
Molecular Formula:2C₆H₃N₃O₇*C₁₇H₂₅N₅S
Molecular Weight:789.696
Hs Code.:
Mol file:144284-46-8.mol

Synonyms:

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Chemical Property of Guanidine, N-[3-(5-methyl-1H-imidazol-4-yl)propyl]-N'-[2-[(phenylmethyl)thio]ethyl]-, compd. with 2,4,6-trinitrophenol (1:2)

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Technology Process of Guanidine, N-[3-(5-methyl-1H-imidazol-4-yl)propyl]-N'-[2-[(phenylmethyl)thio]ethyl]-, compd. with 2,4,6-trinitrophenol (1:2)

There total 3 articles about Guanidine, N-[3-(5-methyl-1H-imidazol-4-yl)propyl]-N'-[2-[(phenylmethyl)thio]ethyl]-, compd. with 2,4,6-trinitrophenol (1:2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1007-54-1
2-benzylsulfanyl-ethylamine

: 144284-46-8
N-(2-Benzylsulfanyl-ethyl)-N'-[3-(5-methyl-1H-imidazol-4-yl)-propyl]-guanidine; compound with picric acid

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 0.25 h / Ambient temperature

2: pyridine / 1 h / Heating

3: 1.) 6 N HCl / 1.) reflux, 2.) conversion into the picrate

With pyridine; hydrogenchloride; In dichloromethane;
DOI:10.1002/ardp.19923250805

Reference yield:

: 112758-77-7
1-Benzoyl-3-(2-benzylsulfanyl-ethyl)-2-phenyl-isourea

: 144284-46-8
N-(2-Benzylsulfanyl-ethyl)-N'-[3-(5-methyl-1H-imidazol-4-yl)-propyl]-guanidine; compound with picric acid

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1 h / Heating

2: 1.) 6 N HCl / 1.) reflux, 2.) conversion into the picrate

With pyridine; hydrogenchloride;
DOI:10.1002/ardp.19923250805

Reference yield:

: 88-89-1
2,4,6-Trinitrophenol

: 144153-33-3
N-Benzoyl-N'-(2-benzylsulfanyl-ethyl)-N''-[3-(5-methyl-1H-imidazol-4-yl)-propyl]-guanidine

: 144284-46-8
N-(2-Benzylsulfanyl-ethyl)-N'-[3-(5-methyl-1H-imidazol-4-yl)-propyl]-guanidine; compound with picric acid

Guidance literature:: With hydrogenchloride; Yield given. Multistep reaction; 1.) reflux, 2.) conversion into the picrate;
DOI:10.1002/ardp.19923250805