Technology Process of 3-Cyclohexene-1-ethanol, 2,2,3-trimethyl-, acetate, (R)-
There total 8 articles about 3-Cyclohexene-1-ethanol, 2,2,3-trimethyl-, acetate, (R)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 78 percent / 40 percent peracetic acid/AcOH, Na2CO3, EDTA tetrasodium salt / toluene / Ambient temperature
2: 75 percent / ZnBr2 / toluene / Heating
3: 97 percent / LiAlH4 / diethyl ether / 1.) reflux, 2.) r.t., 1 h
4: 87 percent / conc. H3PO4 / 2 h / 60 °C
6: 95 percent / hydrogen / Raney-Ni / ethanol / 8 h / Ambient temperature
7: 72 percent / t-BuOK / toluene / 3 h / Heating
8: 70 percent / TsOH / toluene / 2 h / Heating
With
peracetic acid; lithium aluminium tetrahydride; phosphoric acid; potassium tert-butylate; hydrogen; ethylene diamine tetraacetic acid tetrasodium salt; sodium carbonate; toluene-4-sulfonic acid; acetic acid; zinc dibromide;
nickel;
In
diethyl ether; ethanol; toluene;
DOI:10.1002/hlca.19920750507
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 87 percent / conc. H3PO4 / 2 h / 60 °C
3: 95 percent / hydrogen / Raney-Ni / ethanol / 8 h / Ambient temperature
4: 72 percent / t-BuOK / toluene / 3 h / Heating
5: 70 percent / TsOH / toluene / 2 h / Heating
With
phosphoric acid; potassium tert-butylate; hydrogen; toluene-4-sulfonic acid;
nickel;
In
ethanol; toluene;
DOI:10.1002/hlca.19920750507
