(-)-Phleichrome

Base Information

• Chemical Name: (-)-Phleichrome
• CAS No.: 56974-44-8
• UNII: HKX423Y3CK
• Nikkaji Number: J896.756C
• Wikidata: Q27279974,Q105306666

Synonyms:calphostin D;phleichrome;UCN 1028 D;UCN 1028D;UCN-1028D

Chemical Property of (-)-Phleichrome

Chemical Property:

• XLogP3: 4.2
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 10
• Rotatable Bond Count: 8
• Exact Mass: 550.18389715
• Heavy Atom Count: 40
• Complexity: 973

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC(CC1=C2C3=C(C(=C(C4=C3C(=C5C2=C(C(=O)C=C5OC)C(=C1OC)O)C(=CC4=O)OC)O)OC)CC(C)O)O
• Isomeric SMILES: C[C@@H](CC1=C2C3=C(C(=C(C4=C3C(=C5C2=C(C(=O)C=C5OC)C(=C1OC)O)C(=CC4=O)OC)O)OC)C[C@H](C)O)O

Technology Process of (-)-Phleichrome

There total 52 articles about (-)-Phleichrome which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1,12-Bis-((S)-2-hydroxy-propyl)-2,6,7,11-tetramethoxy-4,9-bis-methoxymethoxy-perylene-3,10-dione (133379-36-9) → phleichrome (56974-44-8,77115-15-2,124986-26-1,125411-34-9,127180-30-7,132880-98-9,136374-42-0)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; methanol; water; at 20 ℃; for 0.0333333h;

DOI:10.1016/S0040-4039(00)92105-1

Reference yield:

C32H34O10 → isophleichrome (56974-44-8,77115-15-2,124986-26-1,125411-34-9,127180-30-7,132880-98-9,136374-42-0)

Guidance literature:

With magnesium iodide; In tetrahydrofuran; diethyl ether; for 0.166667h; Inert atmosphere;

DOI:10.1021/ja902324j

Reference yield:

1,12-Bis-((S)-2-hydroxy-propyl)-2,6,7,11-tetramethoxy-4,9-bis-methoxymethoxy-perylene-3,10-dione (133379-36-9) → isophleichrome (56974-44-8,77115-15-2,124986-26-1,125411-34-9,127180-30-7,132880-98-9,136374-42-0)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; methanol; water; at 20 ℃; for 0.0333333h;

DOI:10.1016/S0040-4039(00)92105-1

upstream raw materials:

phleichrome

1,12-Bis-((S)-2-hydroxy-propyl)-2,6,7,11-tetramethoxy-4,9-bis-methoxymethoxy-perylene-3,10-dione

2-bromo-1,5-dimethoxy-3-methylbenzene

2,4-dimethoxy-6-methylbenzoic acid

Downstream raw materials:

hypocrellin-B

isophleichrome

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