Roussin's red salt

Base Information

Chemical Name:Roussin's red salt
CAS No.:58204-17-4
Molecular Formula:Fe2N4 O4 S2 . 2 Na
Molecular Weight:295.8444
Hs Code.:
Mol file:58204-17-4.mol

Synonyms:Ferrate(2-),tetranitrosyldi-m-thioxodi-,(Fe-Fe), disodium (9CI); Disodium tetranitrosyldisulfidodiferrate(2-); Disodiumtetranitrosyldithiodiferrate(2-)

Suppliers and Price of Roussin's red salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Roussin's red salt

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：95.16000
Density:g/cm³
LogP:-0.41988

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Roussin's red salt

There total 1 articles about Roussin's red salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99619-51-9
Roussin's black salt

: 7732-18-5
water

: 1310-73-2
sodium hydroxide

: 58204-17-4
Roussin's red sodium salt

Guidance literature:: In water; byproducts: ammonia; under N2, mixt. of NH4(Fe4S3(NO)7) and 10% NaOH soln. stirred and heated in water bath at 80°C for ca. 4 h; filtered hot, concd., left standing at room temp. overnight, crystals collected, washed with Et2O, dried in vac., purified by dissolution in THF under N2, filtration, evapn. in vac., drying in vac.;

Reference yield: 99.0%

: 58204-17-4
Roussin's red sodium salt

: 894-06-4
triphenyl lead bromide

: 79827-03-5
((C₆H₅)3PbS)2Fe₂(NO)4

Guidance literature:: In tetrahydrofuran; under N2, Ph3PbBr added to stirred soln. of Na(S2Fe2(NO)4)*8H2O in THF, stirred for 2 h; evapd. in vac., chromd. (SiO2, 20% CH2Cl2/pentane), evapd., recrystd. from CH2Cl2/pentane under N2; elem. anal.;

Reference yield: 99.0%

: 58204-17-4
Roussin's red sodium salt

: 894-06-4
triphenyl lead bromide

: ((C₆H₅)3PbS)2Fe₂(NO)4

Guidance literature:: In tetrahydrofuran; byproducts: sodium bromide; room temp., N2 atm. or under vac., stirring, reagent in excess; column chromy., elem. anal.;
DOI:10.1016/S0022-328X(00)80995-X