Benzoic acid, 2-[(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1-oxoundec yl)amino]-

Base Information

• Chemical Name: Benzoic acid, 2-[(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1-oxoundec yl)amino]-
• CAS No.: 144584-05-4
• Molecular Formula: C18H10F17NO3
• Molecular Weight: 611.255
• Mol file: 144584-05-4.mol

Synonyms:

Chemical Property of Benzoic acid, 2-[(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1-oxoundec yl)amino]-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 2-[(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1-oxoundec yl)amino]-

There total 2 articles about Benzoic acid, 2-[(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1-oxoundec yl)amino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoylchloride (89373-67-1) + anthranilic acid (118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4) → 2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoylamino)-benzoic acid (144584-05-4)

Guidance literature:

With pyridine; In tetrahydrofuran; for 1h; Ambient temperature;

DOI:10.1016/S0022-1139(00)82790-6

Reference yield:

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoic acid (34598-33-9) → 2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoylamino)-benzoic acid (144584-05-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / SO₂Cl₂ / 2 h / Heating

2: 94 percent / pyridine / tetrahydrofuran / 1 h / Ambient temperature

With pyridine; sulfuryl dichloride; In tetrahydrofuran;

DOI:10.1016/S0022-1139(00)82790-6

Reference yield:

2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecanoylamino)-benzoic acid (144584-05-4) → 2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-Heptadecafluoro-decyl)-3-phenyl-3H-quinazolin-4-one

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / 1 h / 110 °C

2: 100 percent / ethanol / 4 h / Heating

In ethanol;

DOI:10.1016/S0022-1139(00)82790-6

upstream raw materials:

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoylchloride

anthranilic acid

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoic acid

Refernces