4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundecanoyl chloride

Base Information

Chemical Name:4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundecanoyl chloride
CAS No.:89373-67-1
Molecular Formula:C11H4 Cl F17 O
Molecular Weight:510.578
Hs Code.:2915900090
European Community (EC) Number:625-067-9
DSSTox Substance ID:DTXSID90446276
Nikkaji Number:J641.693D
Wikidata:Q81985976
Mol file:89373-67-1.mol

Synonyms:89373-67-1;4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundecanoyl chloride;(Perfluorooctyl)propanoyl chloride;SCHEMBL3964350;DTXSID90446276;3-(perfluorooctyl)propionyl chloride;4 4 5 5 6 6 ....-Heptadecafluoro-undecan;4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundecanoyl chloride, >=97.0% (GC)

Suppliers and Price of 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundecanoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundecanoyl chloride ≥97.0%(GC)
1 g
$ 194.00

Sigma-Aldrich
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundecanoyl chloride ≥97.0% (GC)
1g-f
$ 184.00

American Custom Chemicals Corporation
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-HEPTADECAFLUOROUNDECANOYL CHLORIDE 95.00%
1G
$ 782.23

Total 4 raw suppliers

Chemical Property of 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundecanoyl chloride

Chemical Property:

Vapor Pressure:0.131mmHg at 25°C
Refractive Index:1.312
Boiling Point:217.687°C at 760 mmHg
Flash Point:85.454°C
PSA：17.07000
Density:1.638g/cm³
LogP:6.54140
XLogP3:6.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:18
Rotatable Bond Count:9
Exact Mass:509.9679212
Heavy Atom Count:30
Complexity:649

Purity/Quality:

98%,99%, ^*data from raw suppliers

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundecanoyl chloride ≥97.0%(GC) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C(CC(C(C(C(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)C(=O)Cl

Technology Process of 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundecanoyl chloride

There total 7 articles about 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundecanoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 34598-33-9
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoic acid

: 89373-67-1
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoylchloride

Guidance literature:: With thionyl chloride; Heating;
DOI:10.1016/0223-5234(92)90020-2

Reference yield:

: 678-39-7
3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-1-decanol

: 89373-67-1
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoylchloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: 88 percent / Et₃N / tetrahydrofuran / 10 h / Heating

2.1: 93 percent / LiBr / acetone / 7 h / Heating

3.1: Mg; I₂ / tetrahydrofuran / 4 h / Heating

3.2: tetrahydrofuran / -6 - 24 °C

4.1: 84 percent / PCl₅ / diethyl ether / 4 h / Heating

With phosphorus pentachloride; iodine; magnesium; triethylamine; lithium bromide; In tetrahydrofuran; diethyl ether; acetone; 3.2: Grignard reaction;
DOI:10.1021/jo010767p

Reference yield:

: 113823-56-6
toluene-4-sulfonic acid 1,1,2,2-tetrahydroperfluorodecyl ester

: 89373-67-1
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoylchloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: 93 percent / LiBr / acetone / 7 h / Heating

2.1: Mg; I₂ / tetrahydrofuran / 4 h / Heating

2.2: tetrahydrofuran / -6 - 24 °C

3.1: 84 percent / PCl₅ / diethyl ether / 4 h / Heating

With phosphorus pentachloride; iodine; magnesium; lithium bromide; In tetrahydrofuran; diethyl ether; acetone; 2.2: Grignard reaction;
DOI:10.1021/jo010767p