[2-[Acetyl-[(4-methylsulfonylphenyl)methyl]amino]-2,2-dichloroethyl] 2,2-dichloroacetate

Base Information

Chemical Name:[2-[Acetyl-[(4-methylsulfonylphenyl)methyl]amino]-2,2-dichloroethyl] 2,2-dichloroacetate
CAS No.:3653-50-7
Molecular Formula:C14H15Cl4NO5S
Molecular Weight:451.155
Hs Code.:
DSSTox Substance ID:DTXSID40190035
Wikidata:Q83062289

Synonyms:M & B 5472;BRN 2824312;C14H15Cl4NO5S;DTXSID40190035;C14-H15-Cl4-N-O5-S

Suppliers and Price of [2-[Acetyl-[(4-methylsulfonylphenyl)methyl]amino]-2,2-dichloroethyl] 2,2-dichloroacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of [2-[Acetyl-[(4-methylsulfonylphenyl)methyl]amino]-2,2-dichloroethyl] 2,2-dichloroacetate

Chemical Property:

Vapor Pressure:2.04E-15mmHg at 25°C
Boiling Point:622.5°Cat760mmHg
Flash Point:330.3°C
Density:1.501g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:450.939554
Heavy Atom Count:25
Complexity:583

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)N(CC1=CC=C(C=C1)S(=O)(=O)C)C(COC(=O)C(Cl)Cl)(Cl)Cl

Technology Process of [2-[Acetyl-[(4-methylsulfonylphenyl)methyl]amino]-2,2-dichloroethyl] 2,2-dichloroacetate

There total 6 articles about [2-[Acetyl-[(4-methylsulfonylphenyl)methyl]amino]-2,2-dichloroethyl] 2,2-dichloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5398-77-6
para-methanesulfonylbenzaldehyde

: 3653-50-7
α,α-Dichlor-N-(2-dichloracetoxy-aethyl)-N-(4-methylsulfonyl-benzyl)-acetamid

Guidance literature:: Multi-step reaction with 3 steps

1: (i) EtOH, (ii) H₂, Raney-Ni

3: Py

With pyridine;
DOI:10.1039/jr9620001420

Reference yield:

: 92244-31-0
(2-Hydroxy-aethyl)-(4-methylsulfon-benzyl)-amin

: 3653-50-7
α,α-Dichlor-N-(2-dichloracetoxy-aethyl)-N-(4-methylsulfonyl-benzyl)-acetamid

Guidance literature:: Multi-step reaction with 2 steps

2: Py

With pyridine;
DOI:10.1039/jr9620001420

Reference yield:

: 3185-99-7
Methyl p-tolyl sulfone

: 3653-50-7
α,α-Dichlor-N-(2-dichloracetoxy-aethyl)-N-(4-methylsulfonyl-benzyl)-acetamid

Guidance literature:: Multi-step reaction with 5 steps

1: Br₂ / Irradiation

2: hexamethylenetetramine

3: (i) EtOH, (ii) H₂, Raney-Ni

5: Py

With pyridine; hexamethylenetetramine; bromine;
DOI:10.1039/jr9620001420